N-叔丁基氧羰基-L-组氨酸甲酯合成路线 (共 12 条)
反应条件
phenyl silane; acetic acid; tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=20°C; deallylation; 3 h;
参考文献
Malanda Kimbonguila; Boucida; Guibe; Loffet
Tetrahedron, 1997 , vol. 53, # 37 p. 12525 - 12538
反应条件
zirconium tetrachloride in acetonitrile T=20°C; 0.166667 h;
参考文献
Sharma; Janardhan Reddy; Sree Lakshmi; Radha Krishna, Palakodety
Tetrahedron Letters, 2004 , vol. 45, # 37 p. 6963 - 6965
反应条件
N,N'-dimethyl-barbituric acid; tetrakis(triphenylphosphine) palladium(0) in dichloromethane deallylation; 8 h; Heating;
参考文献
Malanda Kimbonguila; Boucida; Guibe; Loffet
Tetrahedron, 1997 , vol. 53, # 37 p. 12525 - 12538
反应条件
indium tribromide T=30 - 35°C; 0.5 h;
参考文献
Chankeshwara, Sunay V.; Chakraborti, Asit K.
Synthesis, 2006 , # 16 p. 2784 - 2788
反应条件
1: 90 percent / acetonitrile / 72 h / 40 °C 2: 52 percent / aq. acetic acid; silver acetate / 48 h / 20 °C 3: 89 percent / acetic acid; phenylsilane / tetrakis(triphenylphosphine)palladium / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Malanda Kimbonguila; Boucida; Guibe; Loffet
Tetrahedron, 1997 , vol. 53, # 37 p. 12525 - 12538
反应条件
potassium carbonate in methanol 16 h; Heating;
参考文献
Abdo, Marie-Rose; Joseph, Pascale; Boigegrain, Rose-Anne; Liautard, Jean-Pierre; Montero, Jean-Louis; Koehler, Stephan; Winum, Jean-Yves
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 13 p. 4427 - 4433
反应条件
1: HCl / 16 h / Heating 2: Et3N / methanol / 16 h / Ambient temperature 3: K2CO3 / methanol / 16 h / Heating View Scheme
参考文献
Dancer, Jane E.; Ford, Mark J.; Hamilton, Kenneth; Kilkelly, Michael; Lindell, Stephen D.; O'Mahony, Mary J.; Saville-Stones, Elizabeth A.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 17 p. 2131 - 2136
反应条件
1: Et3N / methanol / 16 h / Ambient temperature 2: K2CO3 / methanol / 16 h / Heating View Scheme
参考文献
Dancer, Jane E.; Ford, Mark J.; Hamilton, Kenneth; Kilkelly, Michael; Lindell, Stephen D.; O'Mahony, Mary J.; Saville-Stones, Elizabeth A.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 17 p. 2131 - 2136
反应条件
thionyl chloride Heating;
参考文献
Chen, Wei-Chuan; Joullie, Madeleine M.
Tetrahedron Letters, 1998 , vol. 39, # 46 p. 8401 - 8404
反应条件
acetic acid; zinc 1.5 h; Ambient temperature;
参考文献
Coyle, Susan; Hallett, Allan; Munns, Michael S.; Young, Geoffrey T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 522 - 528