3-硝基-1,2,4-三氮唑合成路线 (共 29 条)
反应条件
urea; sodium nitrite in water; acetic acid
参考文献
Commissariat a l'Energie Atomique
Patent: US4958027 A1, 1990 ;
反应条件
sodium tungstate; water; dihydrogen peroxide T=20°C; 24 h;
参考文献
Kofman; Paketina
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 8 p. 1125 - 1132
反应条件
XeF2 in acetonitrile T=20°C; 30 h; Yield given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 3.2 p. 662 - 663
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 736 - 738
反应条件
potassium tert-butylate in tetrahydrofuran T=20 - 25°C; 2 h; DMSO as a solvent; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 587 - 588
Zhurnal Organicheskoi Khimii, , vol. 18, # 2 p. 676 - 677
反应条件
potassium tert-butylate in tetrahydrofuran T=20 - 25°C; 2 h; DMSO as a solvent; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 587 - 588
Zhurnal Organicheskoi Khimii, , vol. 18, # 2 p. 676 - 677
反应条件
potassium tert-butylate in tetrahydrofuran T=20 - 25°C; 2 h; DMSO as a solvent; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 587 - 588
Zhurnal Organicheskoi Khimii, , vol. 18, # 2 p. 676 - 677
反应条件
potassium tert-butylate in tetrahydrofuran T=20 - 25°C; 2 h; DMSO as a solvent; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 587 - 588
Zhurnal Organicheskoi Khimii, , vol. 18, # 2 p. 676 - 677
反应条件
XeF2 in acetonitrile T=20°C; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 3.2 p. 662 - 663
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 736 - 738
反应条件
methyl iodide T=3 - 21°C; 1.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 9 p. 1470 - 1475
Zhurnal Organicheskoi Khimii, , vol. 30, # 9 p. 1398 - 1403
反应条件
lithium perchlorate in acetonitrile electrolysis, Ag/0.1N Ag+ reference electrode, E=1.8V; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 1458 - 1461
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1643 - 1646