hydrogenchloride; acetic acid Behandeln des Reaktionsgemisches mit Kaliumhydroxid und anschliessendes Erhitzen;
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Fegley et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4144
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Rohm and Haas Co.
Patent: US2770628 , 1953 ;
Martinez, Gregory R.; Walker, Keith A. M.; Hirschfeld, Donald R.; Maloney, Patrick J.; Yang, Diana S.; Rosenkranz, Roberto P.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 4 p. 890 - 897
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h; regioselective reaction;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358