2-羟基-3-(4-羟基-3-甲氧基苯基)丙酸合成路线 (共 4 条)
反应条件
hydrogenchloride; mercury; zinc in toluene T=120°C; 4 h;
参考文献
Wong; Xu; Chang; Lee
Synthesis, 1992 , # 8 p. 793 - 797
反应条件
D-glucose in dimethyl sulfoxide T=37°C; 5 h; aq. bufferanaerobic atmosphereEnzymatic reaction;
参考文献
Braune, Annett; Bunzel, Mirko; Yonekura, Reiko; Blaut, Michael
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 8 p. 3356 - 3362
反应条件
1: 74 percent / NaOAc / 4 h / 120 °C 2: 1) 3 N HCl, 2) Zn(Hg), 3 N HCl / 1) reflux, 8 h, 2) toluene, 90 deg C, 3 h View Scheme
参考文献
Wong; Xu; Chang; Lee
Synthesis, 1992 , # 8 p. 793 - 797
反应条件
D-glucose in dimethyl sulfoxide T=37°C; aq. bufferanaerobic atmosphereEnzymatic reaction;
参考文献
Braune, Annett; Bunzel, Mirko; Yonekura, Reiko; Blaut, Michael
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 8 p. 3356 - 3362