6-甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 46 条）
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 274, p. 39,46
US2223664 , ;
DE708114 , ;
DRP/DRBP Org.Chem.
DE714848 , ;
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 274, p. 39,46
US2223664 , ;
DE708114 , ;
DRP/DRBP Org.Chem.
DE714848 , ;
参考文献
Journal of the Chemical Society, , p. 689
反应条件
boron trichloride; tetra-(n-butyl)ammonium iodide in dichloromethane T=-78 - 0°C; dealkylation; 1 h;
参考文献
Brooks, Paige R.; Wirtz, Michael C.; Vetelino, Michael G.; Rescek, Diane M.; Woodworth, Graeme F.; Morgan, Bradley P.; Coe, Jotham W.
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9719 - 9721
反应条件
1: With ammonium acetate in methanol T=20°C; 0.5 h; 2: With sodium cyanoborohydride 1 - 2 h; Heating / reflux;
参考文献
JANSSEN PHARMACEUTICA, N.V.
Patent: WO2004/37779 A1, 2004 ;
Location in patent: Page 31 ;
Title/Abstract Full Text Show Details
JANSSEN PHARMACEUTICA, N.V.; Demarest, Keith, T.
Patent: WO2004/37778 A1, 2004 ;
Location in patent: Page 31 ;
反应条件
1: 7 h / 100 °C 2: glucose dehydrogenase; tetrahydroxynaphthalene reductase; D-glucose; β-NADP / isopropyl alcohol / pH 7 / KPi buffer; Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Schaetzle, Michael A.; Flemming, Stephan; Husain, Syed Masood; Richter, Michael; Guenther, Stefan; Mueller, Michael
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2643 - 2646
反应条件
1: 82 percent / (NH4)2CO3 / ethanol; H2O / 18 h / 80 °C 2: 85 percent / Ba(OH)2 / H2O / 24 h / 125 °C View Scheme
参考文献
Obrecht; Spiegler; Schonholzer; Muller; Heimgartner; Stierli
Helvetica Chimica Acta, 1992 , vol. 75, # 5 p. 1666 - 1696
参考文献
A. Christiaens, Societe Anonyme
Patent: US3943172 A1, 1976 ;
反应条件
sodium tetrahydroborate in ethanol T=20°C; 4 h;
参考文献
Tauber, Katharina; Fuchs, Michael; Sattler, Johann H.; Pitzer, Julia; Pressnitz, Desiree; Koszelewski, Dominik; Faber, Kurt; Pfeffer, Jan; Haas, Thomas; Kroutil, Wolfgang
Chemistry - A European Journal, 2013 , vol. 19, # 12 p. 4030 - 4035
