6-甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 46 条）
反应条件
1: thionyl chloride / benzene 2: 88 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 3: 59 percent / diethyl ether / 0.5 h / Ambient temperature 4: 24 percent / acetonitrile / Irradiation View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 458 - 462
反应条件
1: 93 percent / oxalic acid / H2O / 6 h / Heating 2: 1.) formic acid, 30 percent hydrogen peroxide; 2.) 20 percent H2SO4 / 1.) 35 deg C, 2 h, room temp., 12 h; 2.) reflux, 10 h View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 5-6 p. 161 - 166
反应条件
1: KOH, NaOH / 325 °C 2: (i) Na, MeOH, (ii) /BRN= 609209/, dioxane 3: Na, 3-methyl-butan-1-ol 4: aq. HCO2H View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 7, p. 519 - 524
反应条件
1: t-BuOOH, tetrabutylammonium fluoride 2: 8 percent / H3O(1+) View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
反应条件
1: 97 percent / thionyl chloride / 18 h / 25 °C 2: 1.) aluminum chloride / 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, RT, 18 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 6 p. 902 - 921
反应条件
in acetonitrile Irradiation;
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 458 - 462
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
反应条件
1: 86 percent / n-Bu4NHSO4, NaOH, H2O2 / 0.25 h / Ambient temperature 2: 75 percent / 3N HCl / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5201 - 5204
反应条件
aluminium trichloride in dichloromethane 1.) -27 deg C, 30 min, 2.) -10 deg C, 1 h, 3.) 0-5 deg C, 1 h, H2O; further temperatures;
参考文献
Fivush, Adam M.; Strunk, Sanford R.
Synthetic Communications, 1996 , vol. 26, # 8 p. 1623 - 1627
