6-甲氧基-3,4-二氢-1H-2-萘酮合成路线 (共 46 条)
反应条件
hydrogenchloride; ethanol; sodium 1.) reflux, 1 h, 2.) EtOH, reflux, 30 min; Multistep reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 20 p. 2891 - 2898
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C;
参考文献
Fristad, William E.; Bailey, Thomas R.; Paquette, Leo A.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3028 - 3037
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 4 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2831 - 2834
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; Friedel Crafts reaction; 2 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 41 p. 5713 - 5715
反应条件
rhodium (II) acetate in dichloromethane Heating;
参考文献
McKervey, M. Anthony; Tuladhar, Sarbajna M.; Twohig, M. Fiona
Journal of the Chemical Society, Chemical Communications, 1984 , # 2 p. 129 - 130
反应条件
toluene-4-sulfonic acid in benzene 0.25 h; Heating;
参考文献
Hauser, Frank M.; Prasanna, Subbarao
Synthesis, 1980 , # 8 p. 621 - 623
反应条件
meta-chloroperoxybenzoic acid; dichloromethane
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 274, p. 39,46
反应条件
sodium perchlorate; water T=25°C; pH 6.2 - 8.8; kinetic deuterium isotope effect; Product distributionMechanism;
参考文献
Gillilan, Richard E.; Pohl, Terese M.; Whalen, Dale L.
Journal of the American Chemical Society, 1982 , vol. 104, # 16 p. 4482 - 4484
反应条件
aluminium trichloride 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, RT, 18 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 51, # 6 p. 902 - 921
反应条件
1: CH2Cl2 2: CH2Cl2 3: ZnCl2 / CH2Cl2 4: Zn / acetic acid View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 1 p. 117 - 120