1,3-二氢-2-苯并噻吩合成路线 （共 28 条）
反应条件
1: 81 percent / 60percent H2O2, HOAc / 4 h / 0 °C 2: 40 percent / CH2Cl2 / 7 h / Ambient temperature 3: 77 percent / NEt3 / CH2Cl2 / 10 h / Ambient temperature View Scheme
参考文献
Kawabata, Kohsuke; Goto, Hiromasa
Journal of Materials Chemistry, 2012 , vol. 22, # 44 p. 23514 - 23524
反应条件
1: Cl2, H2O 2: N2H4*H2O / CH2Cl2 3: Cl2 / CH2Cl2 View Scheme
参考文献
King,J.F. et al.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 943 - 955
反应条件
dihydrogen peroxide; Corallina officinalis vanadium-containing bromoperoxidase in phosphate buffer T=25°C; Oxidation; pH=6.5; 16 h;
参考文献
Andersson, Malin; Willetts, Andrew; Allenmark, Stig
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8455 - 8458
反应条件
hexaphenyldistannathiane, bis(triphenyltin)sulfide; sodium iodide in butanone
6 h; Heating;
参考文献
Steliou, Kosta; Salama, Paul; Corriveau, Jean
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4969 - 4971
反应条件
sodium hydride in N,N-dimethyl-formamide
T=80°C; 4 h;
参考文献
Yamato, M.; Takeuchi, Y.; Hattori, K.; Hashigaki, K.
Synthesis, 1982 , # 12 p. 1014 - 1015
反应条件
in diethyl ether
T=20°C; Irradiation;
参考文献
Bailey, R. J.; Card, P. J.; Shechter, H.
Journal of the American Chemical Society, 1983 , vol. 105, # 19 p. 6096 - 6103
反应条件
in chlorobenzene
Heating;
参考文献
Bailey, R. J.; Card, P. J.; Shechter, H.
Journal of the American Chemical Society, 1983 , vol. 105, # 19 p. 6096 - 6103
反应条件
iodine; silica gel in diethyl ether; dichloromethane
参考文献
Rys, Andrzej Z.; Abu-Yousef, Imad A.; Harpp, David N.
Tetrahedron Letters, 2008 , vol. 49, # 47 p. 6670 - 6673
反应条件
S(MgBr)2 in tetrahydrofuran
4 h; Heating;
参考文献
Nedugov, A. N.; Pavlova, N. N.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 7.1 p. 1103 - 1104
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 7 p. 1401 - 1402
反应条件
sodium sulfide nonahydride in ethanol
0.666667 h; Reflux;
参考文献
Kawabata, Kohsuke; Goto, Hiromasa
Journal of Materials Chemistry, 2012 , vol. 22, # 44 p. 23514 - 23524
