6-甲氧基-1,2,3,4-四氢-萘-2-羧酸合成路线 （共 19 条）
反应条件
1: hydrogen fluoride
2: palladium/charcoal; ethanol / Hydrogenation
3: aqueous hydrochloric acid; acetic acid
View Scheme
参考文献
Price; Kaplan
Journal of the American Chemical Society, 1944 , vol. 66, p. 477
反应条件
ammonia; lithium in tetrahydrofuran
0.5 h;
参考文献
Murthy, A. Radhakrishna; Sundar, N. Shyama; Rao, G. S. R. Subba
Tetrahedron, 1982 , vol. 38, # 18 p. 2831 - 2836
反应条件
1: NaBH4 / methanol
2: KHSO4 / 0.08 h / 165 - 170 °C
3: 99 percent / Mg, methanol / 2 h
4: 100 percent / KOH / methanol / 22 h / Heating
View Scheme
参考文献
Chatterjee, Amareshwar; Roy, Dinabandhu; Chatterjee, S.K.
Synthesis, 1981 , # 6 p. 449 - 451
反应条件
1: 99 percent / Mg, methanol / 2 h
2: 100 percent / KOH / methanol / 22 h / Heating
View Scheme
参考文献
Chatterjee, Amareshwar; Roy, Dinabandhu; Chatterjee, S.K.
Synthesis, 1981 , # 6 p. 449 - 451
反应条件
1: KHSO4 / 0.08 h / 165 - 170 °C
2: 99 percent / Mg, methanol / 2 h
3: 100 percent / KOH / methanol / 22 h / Heating
View Scheme
参考文献
Chatterjee, Amareshwar; Roy, Dinabandhu; Chatterjee, S.K.
Synthesis, 1981 , # 6 p. 449 - 451
反应条件
T=200°C; P=128714 Torr; Hydrogenation;
参考文献
Dauben et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1393,1397
反应条件
sodium; hydrazine hydrate; diethylene glycol
参考文献
Jacques; Horeau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 228, p. 1873
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Horeau; Jacques
Bulletin de la Societe Chimique de France, 1950 , p. 512,516
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 22, p. 1873,1875
反应条件
1: aqueous NaOH
2: isoamyl alcohol; sodium
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参考文献
Horeau; Jacques
Bulletin de la Societe Chimique de France, 1950 , p. 512,516
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 22, p. 1873,1875
反应条件
1: CH2Cl2; diethyl ether / 15 h / -20 °C
2: Rh(OAc)2 / CH2Cl2 / 0.08 h / Heating
View Scheme
参考文献
Morris, Jonathan C.; Mander, Lewis N.; Hockless, David C. R.
Synthesis, 1998 , # SPEC. ISS. APR. p. 455 - 467
