6-甲氧基-1,2,3,4-四氢-萘-2-羧酸合成路线 (共 19 条)
参考文献
Price; Kaplan
Journal of the American Chemical Society, 1944 , vol. 66, p. 477
反应条件
hydrogen; palladium on activated charcoal in methanol
P=760 Torr; Ambient temperature;
参考文献
Itoh; Miyake; Tanabe; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2006 - 2015
反应条件
ammonia; lithium in tetrahydrofuran
0.5 h;
参考文献
Murthy, A. Radhakrishna; Sundar, N. Shyama; Rao, G. S. R. Subba
Tetrahedron, 1982 , vol. 38, # 18 p. 2831 - 2836
反应条件
potassium hydroxide in methanol
22 h; Heating;
参考文献
Chatterjee, Amareshwar; Roy, Dinabandhu; Chatterjee, S.K.
Synthesis, 1981 , # 6 p. 449 - 451
反应条件
1: 81 percent / Ag2O / ethanol; H2O / 20 °C
2: 91 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Dey, Satyajit; Mal, Dipakranjan
Tetrahedron Letters, 2005 , vol. 46, # 33 p. 5483 - 5486
反应条件
1: 72 percent / POCl3 / 100 °C
2: 81 percent / Ag2O / ethanol; H2O / 20 °C
3: 91 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Dey, Satyajit; Mal, Dipakranjan
Tetrahedron Letters, 2005 , vol. 46, # 33 p. 5483 - 5486
反应条件
1: 96 percent / NaBH4 / methanol / 20 °C
2: 72 percent / POCl3 / 100 °C
3: 81 percent / Ag2O / ethanol; H2O / 20 °C
4: 91 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Dey, Satyajit; Mal, Dipakranjan
Tetrahedron Letters, 2005 , vol. 46, # 33 p. 5483 - 5486
反应条件
hydrogenchloride; acetic acid
参考文献
Price; Kaplan
Journal of the American Chemical Society, 1944 , vol. 66, p. 477
参考文献
Dauben et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1393,1397
反应条件
1: palladium/charcoal; ethanol / Hydrogenation
2: aqueous hydrochloric acid; acetic acid
View Scheme
参考文献
Price; Kaplan
Journal of the American Chemical Society, 1944 , vol. 66, p. 477