S-苄基-S-苯基-N-对甲苯磺酰硫亚胺合成路线 (共 6 条)
反应条件
copper trifluoromethanesulfonate in acetonitrile T=25°C; 48 h;
参考文献
Takada, Hiroya; Nishibayashi, Yoshiaki; Ohe, Kouichi; Uemura, Sakae
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 120-121, p. 363 - 364
反应条件
in acetonitrile T=20°C; 16 h;
参考文献
Marzinzik; Sharpless
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 594 - 596
反应条件
1: With [bis(acetoxy)iodo]benzene in dichloromethane Oxidation; 0.5 h; 2: With triethylamine Condensation; 1 h;
参考文献
Ou, Wei; Chen, Zhen-Chu
Synthetic Communications, 1999 , vol. 29, # 24 p. 4443 - 4449
反应条件
copper trifluoromethanesulfonate in dichloromethane; toluene T=20°C; 48 h;
参考文献
Meprathu, Bindu V.; Protasiewicz, John D.
Tetrahedron, 2010 , vol. 66, # 31 p. 5768 - 5774
反应条件
1: 48 percent / KOH / methanol / 0 - 20 °C 2: 82 percent / CuOTf / acetonitrile / 48 h / 25 °C View Scheme
参考文献
Takada, Hiroya; Nishibayashi, Yoshiaki; Ohe, Kouichi; Uemura, Sakae; Baird, Charlotte P.; Sparey, Tim J.; Taylor, Paul C.
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6512 - 6518
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; chloroform 2 h; Ambient temperature;
参考文献
Furukawa, Naomichi; Hoshino, Kimie; Morishita, Tsuyoshi; Oae, Shigeru
Synthesis, 1984 , # 4 p. 317 - 319