1: With potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=90°C; 0.333333 h; microwave irradiation; 2: With hydrogenchloride in water 0.166667 h; Further stages.;
1: With diisobutylaluminium hydride in toluene T=-78°C; 1 h; 2: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; N-chloro-succinimide; potassium carbonate in dichloromethane; water
water; silver hexafluoroantimonate in tetrahydrofuran T=60°C; Meyer-Schuster rearrangement; 8 h;
参考文献
Marion, Nicolas; Carlqvist, Peter; Gealageas, Ronan; De Fremont, Pierre; Maseras, Feliu; Nolan, Steven P.
Chemistry - A European Journal, 2007 , vol. 13, # 22 p. 6437 - 6451
