9,10-二(4-甲氧苯基)蒽合成路线 (共 22 条)
反应条件
sodium dihydrogenphosphate; potassium iodide in acetic acid 2 h; Heating;
参考文献
Smet, Mario; Van Dijk, Joachim; Dehaen, Wim
Tetrahedron, 1999 , vol. 55, # 25 p. 7859 - 7874
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; toluene Suzuki-Miyaura cross-coupling reaction; Heating;
参考文献
Kotha, Sambasivarao; Ghosh, Arun Kumar; Deodhar, Kodand Dinkar
Synthesis, 2004 , # 4 p. 549 - 557
反应条件
tetra-n-butylammonium tetrafluoroborate; zinc in dichloromethane; trifluoroacetic acid 1.) electrolysis, 2.) 2 h;
参考文献
Svanholm, Ulla; Parker, Vernon D.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 1 p. 5 - 14
参考文献
Chemistry - An Asian Journal, , vol. 8, # 11 p. 2588 - 2591
反应条件
1.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C / |Inert atmosphere 1.2: 12 h / 20 °C / |Inert atmosphere 2.1: toluene-4-sulfonic acid / dichloromethane / 12 h / 20 °C 3.1: hexafluoroisopropyl alcohol / 0.17 h / 0 °C / |Inert atmosphere 4.1: biscyclopentadienyliron(II) / 1 h / 0 °C View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 8, # 11 p. 2588 - 2591
反应条件
magnesium; palladium diacetate 1.) ether; 2.) ether, THF, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 516, # 1-2 p. 225 - 232
反应条件
(electrochemical oxidation);
参考文献
Journal of the American Chemical Society, , vol. 98, # 10 p. 2942 - 2946
反应条件
in o-xylene T=80°C; Kinetics; Further Variations:Temperatures;
参考文献
Chemical Communications, , # 15 p. 1771 - 1773
反应条件
Bu4NFBF4 in dichloromethane; trifluoroacetic acid T=11°C; Rate constant;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 34, # 1 p. 5 - 14
反应条件
acetone; copper dichloride
参考文献
Chemistry and Industry (London, United Kingdom), , p. 360
Journal of Organic Chemistry, , vol. 29, p. 26,28