4-(氯甲基)-1,3-二氧戊环-2-酮合成路线 （共 29 条）
反应条件
tributylbenzylphosphonium chloride in various solvent(s)
T=100°C; 24 h;
参考文献
Nishikubo, Tadatomi; Shiina, Atsushi; Isobe, Naoki
Chemistry Letters, 1988 , # 10 p. 1605 - 1608
反应条件
[Ru(TPP)(O)2]; oxygen; tetra-(n-butyl)ammonium iodide in dichloromethane
T=30°C; P=12001.2 Torr; 48 h; Autoclave; chemoselective reaction;
参考文献
Bai, Dongsheng; Jing, Huanwang
Green Chemistry, 2010 , vol. 12, # 1 p. 39 - 41
反应条件
bromine trifluoride in chloroform
T=0°C; Title compound not separated from byproducts.;
参考文献
Hagooly, Youlia; Rozen, Shlomo
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6780 - 6783
反应条件
in dichloromethane
T=-78 - 20°C; Cyclization;
参考文献
Bredikhin; Pashagin; Strunskaya; Gubaydullin; Litvinov; Bredikhina
Russian Chemical Bulletin, 1999 , vol. 48, # 11 p. 2086 - 2090
反应条件
benzyltrimethylammonium bicarbonate
T=120 - 150°C; P=36775.4 Torr;
参考文献
Jefferson Chem. Co.
Patent: US2873282 , 1952 ;
参考文献
Hagooly, Youlia; Rozen, Shlomo
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6780 - 6783
反应条件
triethylamine
Cyclization;
参考文献
Bredikhin; Pashagin; Strunskaya; Gubaydullin; Litvinov; Bredikhina
Russian Chemical Bulletin, 1999 , vol. 48, # 11 p. 2086 - 2090
参考文献
Contardi; Ercoli
Gazzetta Chimica Italiana, 1934 , vol. 64, p. 524
反应条件
water in tetrahydrofuran
参考文献
Huntsman Petrochemical Corporation
Patent: US2002/38041 A1, 2002 ;
