4-硝基苯基2,3,4-三-O-乙酰基-beta-D-吡喃木糖合成路线 (共 5 条)
反应条件
potassium carbonate in acetone Ambient temperature;
参考文献
Takeo; Ohguchi; Hasegawa; Kitamura
Carbohydrate Research, 1995 , vol. 277, # 2 p. 231 - 244
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: sodium acetate / |Reflux 2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: αXylF; pNP β-D-xylopyranoside With Bhxglycosynthase E334G mutant T=20°C; pH=7; 24 h; aq. phosphate bufferEnzymatic reaction; 2: acetic anhydride With pyridine; 4-(N,N-dimethlyamino)pyridine T=20°C; 16 h;
参考文献
Goddard-Borger, Ethan D.; Fiege, Brigitte; Kwan, Emily M.; Withers, Stephen G.
ChemBioChem, 2011 , vol. 12, # 11 p. 1703 - 1711
反应条件
methanol; sodium methylate 5 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 277, # 2 p. 231 - 244