3-叔丁基-2-羟基苯甲醛合成路线 (共 24 条)
反应条件
triethylamine; magnesium chloride in acetonitrile 5 h; Heating;
参考文献
Gisch, Nicolas; Balzarini, Jan; Meier, Chris
Journal of Medicinal Chemistry, 2007 , vol. 50, # 7 p. 1658 - 1667
反应条件
sodium hydroxide in chloroform
参考文献
Ortho Pharmaceutical Corporation
Patent: US5942532 A1, 1999 ;
反应条件
hydrogenchloride 2 h;
参考文献
Journal of Chemical Research, Miniprint, , # 7 p. 743 - 757
反应条件
potassium meta-periodate; sulfuric acid in ethanol
参考文献
Synthesis, , p. 624 - 625
反应条件
1.1: N,N,N',N'-tetramethylethylenediamine; n-BuLi / hexane; diethyl ether / 0 °C 1.2: hexane; diethyl ether 2.1: 1.2 g / aq. HCl / tetrahydrofuran / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 16 p. 4433 - 4451
反应条件
1: LiAlH4 / diethyl ether 2: aq. KIO4, H2SO4 / ethanol View Scheme
参考文献
Synthesis, , p. 624 - 625
反应条件
sodium hydroxide in ethanol; water 1 h; Heating;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 15 p. 1813 - 1819
反应条件
1.1: NaH / tetrahydrofuran; various solvent(s) / 0 °C 2.1: N,N,N',N'-tetramethylethylenediamine; n-BuLi / hexane; diethyl ether / 0 °C 2.2: hexane; diethyl ether 3.1: 1.2 g / aq. HCl / tetrahydrofuran / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 16 p. 4433 - 4451
反应条件
Miyazaki-Newman-Kwart rearrangement; 0.0333333 h; Microwave irradiationNeat (no solvent);
参考文献
European Journal of Organic Chemistry, , # 28 p. 5636 - 5640