(S)-(+)-1,3-丁二醇合成路线 （共 31 条）
反应条件
Ru2Cl4-(S)-(2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2*NEt3; hydrogen in methanol T=50°C; P=38000 Torr; 24 h;
参考文献
Shao, Liming; Takeuchi, Kasumi; Ikemoto, Makoto; Kawai, Toshiyasu; Ogasawara, Masamichi; et al.
Journal of Organometallic Chemistry, 1992 , vol. 435, # 1.2 p. 133 - 147
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Ambient temperature;
参考文献
Larcheveque; Mambu; Petit
Synthetic Communications, 1991 , vol. 21, # 22 p. 2295 - 2300
反应条件
hydrogen; palladium on activated charcoal in methanol T=45°C; 14 h;
参考文献
Frick; Klassen; Bathe; Abramson; Rapoport
Synthesis, 1992 , # 7 p. 621 - 623
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 10 h;
参考文献
Yang, Dan; Zhang, Yu-Hui; Li, Bing; Zhang, Dan-Wei
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7577 - 7581
反应条件
lithium aluminium tetrahydride in diethyl ether 6 h;
参考文献
Besse, Pascale; Ciblat, Stephane; Canet, Jean-Louis; Troin, Yves; Veschambre, Henri
Tetrahedron Asymmetry, 1999 , vol. 10, # 11 p. 2213 - 2224
反应条件
hydrogen; RuCl2[(R)-BINAP] in ethanol P=53200 Torr; 42 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 110, # 2 p. 629 - 631
反应条件
hydrogenchloride in methanol 14 h; Ambient temperature;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Kagamihara, Yasuhiro; Tanaka, Sachi; Inoue, Atsushi; Oku, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1412 - 1421
反应条件
hydrogen; potassium carbonate; palladium on activated charcoal in methanol P=2280 Torr;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 17 p. 1181 - 1182
反应条件
sodium tetrahydroborate in 1-methyl-pyrrolidin-2-one; methanol T=4°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Organic Letters, , vol. 10, # 24 p. 5581 - 5583
反应条件
RuH(η1-BH4)(dppp)((R,R)-dpen); hydrogen in tetrahydrofuran T=80°C; P=37503.8 Torr; 16 h; Autoclave;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 1 p. 92 - 96
