(S)-4-异丙基恶唑-2,5-二酮合成路线 (共 34 条)
反应条件
in tetrahydrofuran T=40°C; 1.5 h;
参考文献
Allen; Hamaker; La Loggia; Cook
Synthetic Communications, 1992 , vol. 22, # 14 p. 2077 - 2102
反应条件
carbon in tetrahydrofuran T=55°C; 0.666667 h;
参考文献
Katakai, Ryoichi; Iizuka, Yasuko
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 715 - 716
反应条件
phosphorus trichoride in dichloromethane T=0°C; 2 h;
参考文献
Akssira; Boumzebra; Kasmi; Dahdouh; Roumestant; Viallefont
Tetrahedron, 1994 , vol. 50, # 30 p. 9051 - 9060
反应条件
N,N-dimethyl-formamide in dichloromethane T=0 - 20°C;
参考文献
Mobashery, Shahriar; Johnston, Michael
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2200 - 2202
反应条件
hydrogenchloride in dichloromethane T=0°C;
参考文献
Benoiton, N. Leo; Chen, Francis M. F.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 384 - 389
反应条件
nitrogen in tetrahydrofuran; toluene
参考文献
Hamilton, Andrew D.; Ernst, Justin; Orner, Brendan P.
Patent: US2003/8882 A1, 2003 ;
反应条件
phosphorus tribromide in diethyl ether
参考文献
Itoh, Osamu; Honnami, Toshiya; Amano, Akira; Murata, Kouichi; Koichi, Youta; Sugita, Toshio
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7334 - 7338
反应条件
N-ethyl-N,N-diisopropylamine; PyCloP in dichloromethane 3 h; Ambient temperature;
参考文献
Frerot, Eric; Coste, Jacques; Poncet, Joel; Jouin, Patrick; Castro, Bertrand
Tetrahedron Letters, 1992 , vol. 33, # 20 p. 2815 - 2816
参考文献
Colonna, Stefano; Molinari, Henriette; Banfi, Stefano; Julia, Sebastian; Masana, Jaume; Alvarez, Angel
Tetrahedron, 1983 , vol. 39, # 9 p. 1635 - 1642
反应条件
1: 75.2 percent / aq. NaOH 2: 67.2 percent / PBr3 / diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 28 p. 7334 - 7338