5-苯基-4-戊炔-1-醇合成路线 （共 19 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine in tetrahydrofuran T=20°C; 12 h;
参考文献
Seiders II, John R.; Wang, Lijun; Floreancig, Paul E.
Journal of the American Chemical Society, 2003 , vol. 125, # 9 p. 2406 - 2407
反应条件
toluene-4-sulfonic acid in methanol T=70°C; 96 h;
参考文献
Fuji, Koji; Morimoto, Tsumoru; Tsutsumi, Ken; Kakiuchi, Kiyomi
Chemical Communications, 2005 , # 26 p. 3295 - 3297
反应条件
1: phenylacetylene With n-butyllithium 2: trimethylene oxide With boron trifluoride diethyl etherate
参考文献
Wessig, Pablo; Mueller, Gunnar; Kuehn, Andreas; Herre, Robert; Blumenthal, Haiko; Troelenberg, Stefanie
Synthesis, 2005 , # 9 art. no. C01705SS, p. 1445 - 1454
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide T=100°C; Sonogashira coupling; 12 h;
参考文献
Hwang, Lee Kyoung; Na, Youngim; Lee, Junseong; Do, Youngkyu; Chang, Sukbok
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6166 - 6169
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine in triethylamine T=80°C;
参考文献
Brimble, Margaret A; Pavia, Gabrielle S; Stevenson, Ralph J
Tetrahedron Letters, 2002 , vol. 43, # 9 p. 1735 - 1738
反应条件
potassium carbonate; AgCl; tetrakis(trimethylphosphane)palladium(0) in methanol; N,N-dimethyl-formamide T=40°C;
参考文献
Halbes, Ulla; Pale, Patrick
Tetrahedron Letters, 2002 , vol. 43, # 11 p. 2039 - 2042
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=60°C; 2 h;
参考文献
Okutani, Masaru; Mori, Yuji
Journal of Organic Chemistry, 2009 , vol. 74, # 1 p. 442 - 444
反应条件
toluene-4-sulfonic acid in ethanol; hexane
反应条件
methanol; potassium hydroxide Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 1084 - 1089
反应条件
1: NaI / acetone 3: KOH / aq. ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 37, # 17 p. 2782 - 2784
