1,2,4-苯三羧酸三甲酯合成路线 （共 45 条）
反应条件
platinum on activated charcoal in m-xylene 96 h; Reflux;
参考文献
AMYRIS, INC.; SCHWEITZER, Dirk, Ph.D.
Patent: WO2012/82725 A1, 2012 ;
Location in patent: Page/Page column 39 ;
反应条件
boron trifluoride T=65°C; 0.333333 h;
参考文献
Jaoui; Kleindienst; Lewandowski; Edney
Analytical Chemistry, 2004 , vol. 76, # 16 p. 4765 - 4778
反应条件
bis(1,5-cyclooctadiene)nickel (0); triphenylphosphine in toluene T=23°C; 1 h; Inert atmosphereGlovebox; regioselective reaction;
参考文献
Rodrigo, Sanjeewa K.; Powell, Israel V.; Coleman, Michael G.; Krause, Jeanette A.; Guan, Hairong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 44 p. 7653 - 7657
反应条件
bis(allyl)-ruthenium(IV) dimer in methanol; water T=75°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 47 p. 15094 - 15095
反应条件
5 Pd(II)/C(eggshell) in diethylene glycol dimethyl ether 27 h; RefluxInert atmosphere;
参考文献
US2010/314243 A1, ;
Page/Page column 31 ;
反应条件
T=160°C; 19 h; Pressure tube;
参考文献
US2010/314243 A1, ;
Page/Page column 24 ;
反应条件
in 1,3,5-trimethyl-benzene T=220°C; 8 h;
参考文献
Chittimalla, Santhosh Kumar; Shiao, Hui-Yi; Liao, Chun-Chen
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 11 p. 2267 - 2277
反应条件
in methanol; dichloromethane T=23°C; 22 h; Yields of byproduct given;
参考文献
Castano, Ana M.; Echavarren, Antonio M.; Lopez, Javier; Santos, Amelia
Journal of Organometallic Chemistry, 1989 , vol. 379, p. 171 - 176
反应条件
1: iodine / acetonitrile / 36 h / Reflux; Ambient light 2: sulfuric acid / 16 h / Reflux 3: hydroquinone / m-xylene / 72 h / Inert atmosphere; Reflux 4: oxygen / platinum on carbon / m-xylene / 96 h / Reflux View Scheme
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Tarnchompoo, Bongkoch; Thebtaranonth, Chachanat; Thebtaranonth, Yodhathai
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6671 - 6674
