N-(6-溴己基)邻苯二甲酰亚胺合成路线 （共 43 条）
反应条件
phosphorus tribromide in toluene
参考文献
Bristol-Myers Squibb Company
Patent: US5583146 A1, 1996 ;
US 5583146 A
反应条件
phosphorus tribromide in toluene T=110°C;
参考文献
Neelakantan, Sundar; Surjawan, Iwan; Karacelik, Huseyin; Hicks, Clair L.; Crooks, Peter A.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 19 p. 5722 - 5726
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Loska, Rafal; Janiga, Anita; Gryko, Dorota
Journal of Porphyrins and Phthalocyanines, 2013 , vol. 17, # 1-2 p. 104 - 117
反应条件
octadecyltributylphosphonium bromide in benzene T=80°C; 4 h;
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Abdrakhmanov, I. B.; Aripova, S. F.
Chemistry of Natural Compounds, 1988 , vol. 24, # 1 p. 66 - 70
Khimiya Prirodnykh Soedinenii, 1988 , vol. 24, # 1 p. 76 - 82
反应条件
lithium bromide in acetone T=20°C;
参考文献
Albert-Seifried, Sebastian; Finlayson, Chris E.; Laquai, Frederic; Friend, Richard H.; Swager, Timothy M.; Kouwer, Paul H. J.; Juricek, Michal; Kitto, Heather J.; Valster, Sanne; Nolte, Roeland J. M.; Rowan, Alan E.
Chemistry - A European Journal, 2010 , vol. 16, # 33 p. 10021 - 10029
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Kowalski, Piotr; Mitka, Katarzyna; Jaskowska, Jolanta; Duszynska, Beata; Bojarski, Andrzej J.
Archiv der Pharmazie, 2013 , vol. 346, # 5 p. 339 - 348
反应条件
in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
WAKAMOTO PHARMACEUTICAL CO., LTD.
Patent: WO2006/51851 A1, 2006 ;
Location in patent: Page/Page column 77 ;
反应条件
1: potassium hydroxide / ethanol; water / Reflux 2: N,N-dimethyl-formamide / 12 h / 100 °C View Scheme
参考文献
Organic Letters, , vol. 13, # 4 p. 764 - 767
反应条件
1: toluene / Heating 2: 68.1 g / PBr3 / toluene / 100 °C View Scheme
参考文献
Synthetic Communications, , vol. 15, # 14 p. 1277 - 1290
反应条件
1: dimethylformamide / 80 °C 2: CBr4; PPh3 / acetonitrile / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 16 p. 4347 - 4351
