Giumanini, Angelo G.; Verardo, Giancarlo; Gorassini, Fausto; Strazzolini, Paolo
Recueil des Travaux Chimiques des Pays-Bas, 1995 , vol. 114, # 7 p. 311 - 316
in hexane byproducts: LiF; dropping a soln. of 2,4,6-tri-t-butylphenyl-difluoroborane in n-hexane to a suspension of freshly lithiated 2,6-di(isopropyl)phenylamine in n-hexane cooled with ice (under N2) followed by refluxing for 3 h; removal of the solvent under reduced pressure and subliming the iminoborane from the residue in anoil pump vacuum, elem. anal.;
参考文献
Geschwentner, M.; Elter, G.; Meller, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1993 , vol. 619, p. 1474 - 1478