N-苄氧羰基-D-苯丙氨酸合成路线 （共 60 条）
反应条件
Aspergillus niger lipase; sodium acetate buffer in diethyl ether Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 22 p. 3719 - 3733
反应条件
in various solvent(s) T=25°C; effect of the catalyst (CBZ-L-Leu-L-Hys-poly(ethyleneimine)s) on the stereoselectivity of hydrolysis; KineticsProduct distribution;
参考文献
Chemistry Letters, , p. 429 - 432
反应条件
1: aq. HCl / 20 h / Heating 2: NaOH; NaHCO3 / H2O / 63 h View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 17, # 18 p. 2667 - 2671
反应条件
1: 70 percent / NEt3 / CH2Cl2 / 4 h / 0 °C 2: Jones' reagent / acetone / 3 h / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 535 - 540
反应条件
sodium hydroxide; sodium hydrogencarbonate in water 63 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 18 p. 2667 - 2671
反应条件
resolved on amylose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Chemistry Letters, , p. 1125 - 1128
反应条件
Multistep reaction; the possibility of the application of the new PetOH protecting group in peptide synthesis was investigated via the rate of racemization;
参考文献
Tetrahedron Letters, , vol. 25, # 36 p. 3971 - 3974
反应条件
1: p-toluolsulfonic acid / 1,1,1-trichloro-ethane / 18 h / Heating 2: 1) K-hexamethyldisilazide / 1) THF-toluene, -78 deg C, 5 min, 2) warming up to rt. 3: 1N NaOH / methanol / Ambient temperature 4: H2 / 10percent Pd/C / methanol / 2 h / 206.9 Torr View Scheme
参考文献
Karady, Sandor; Amato, Joseph S.; Weinstock, Leonard M.
Tetrahedron Letters, 1984 , vol. 25, # 39 p. 4337 - 4340
反应条件
hydrogen; palladium on activated charcoal in methanol 2 h;
参考文献
Szymanski, Wiktor; Ostaszewski, Ryszard
Tetrahedron Asymmetry, 2006 , vol. 17, # 18 p. 2667 - 2671
反应条件
1: p-toluolsulfonic acid / 1,1,1-trichloro-ethane / 18 h / Heating 2: 1) K-hexamethyldisilazide / 1) THF-toluene, -78 deg C, 5 min, 2) warming up to rt. 3: 1N NaOH / methanol / Ambient temperature 4: H2 / 10percent Pd/C / methanol / 2 h / 2068.6 Torr / Ambient temperature View Scheme
参考文献
Karady, Sandor; Amato, Joseph S.; Weinstock, Leonard M.
Tetrahedron Letters, 1984 , vol. 25, # 39 p. 4337 - 4340
