N-苄氧羰基-D-苯丙氨酸合成路线 （共 60 条）
反应条件
jones' reagent in acetone T=0°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 535 - 540
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone Yield given;
参考文献
Journal of Organic Chemistry, , vol. 50, # 3 p. 417 - 419
反应条件
sodium hydrogencarbonate; sodium carbonate in water; acetonitrile T=50°C; Substitution; pH=9.5; 1 h;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 43, # 5 p. 449 - 461
反应条件
1: 64 percent / N-chlorosuccinimide, Et3N / methanol / 0 °C 2: 1.) O3, 2.) (CH3)2S / 1.) CH2Cl2, CH3OH, -78 deg C, 2.) CH2Cl2, CH3OH, from -78 deg C to 25 deg C 3: CrO3, H2SO4 / H2O; acetone View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 3 p. 417 - 419
反应条件
1: 1.) O3, 2.) (CH3)2S / 1.) CH2Cl2, CH3OH, -78 deg C, 2.) CH2Cl2, CH3OH, from -78 deg C to 25 deg C 2: CrO3, H2SO4 / H2O; acetone View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 3 p. 417 - 419
反应条件
S-1-methylheptanol; borate buffer; water; Bis-2-octyl sodium sulphosuccinate; sodium hydroxide in n-heptane T=25°C; kD; Rate constant;
参考文献
Tetrahedron, , vol. 43, # 1 p. 77 - 84
反应条件
sodium hydroxide in methanol 2 h; Ambient temperature;
参考文献
Journal of Antibiotics, , vol. 49, # 9 p. 890 - 899
反应条件
1: 74 percent / BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / 21 h / -55 °C 2: 85 percent / aq. CF3CO2H / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 35 p. 7679 - 7692
反应条件
1: Et3N / CHCl3 / 1.) 0 deg C, 20 min, 2.) room temperature, 2 h 2: 1 N NaOH / methanol / 2 h / Ambient temperature View Scheme
参考文献
Journal of Antibiotics, , vol. 49, # 9 p. 890 - 899
反应条件
1: Et3N / CHCl3 / 1.) 0 deg C, 20 min, 2.) room temperature, 2 h 2: 1 N NaOH / methanol / 2 h / Ambient temperature View Scheme
参考文献
Journal of Antibiotics, , vol. 49, # 9 p. 890 - 899
