[4-(苯基甲氧基)苯基]苯甲酸酯合成路线 （共 6 条）
反应条件
hydrogenchloride; potassium hydroxide; tetrabutylammomium bromide in toluene
参考文献
Sumitomo Chemical Company, Limited
Patent: US5872137 A1, 1999 ;
反应条件
[bis(acetoxy)iodo]benzene; triethylamine; 1,1'-carbonyldiimidazole in dichloromethane T=20°C; 3 h;
参考文献
Ruso, Jayaraman Sembian; Rajendiran, Nagappan; Kumaran, Rajendran Senthil
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2345 - 2347
反应条件
1: H2 / Pd-C / ethanol 2: MeSO2Cl 3: (i) (catalytic hydrogenation), (ii) NaNO2, H2SO4, (iii) aq. NaI, I2, CHCl3, urea 4: aq. HCl / acetic acid View Scheme
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
反应条件
1: H2 / Pd-C / ethanol 2: MeSO2Cl 3: (i) (catalytic hydrogenation), (ii) NaNO2, H2SO4, (iii) aq. NaI, I2, CHCl3, urea 4: aq. HCl / acetic acid View Scheme
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
反应条件
1: H2 / Pd-C / ethanol
2: (i) (nitration), (ii) /BRN= 2050596/, MeSO2Cl
3: (i) (catalytic hydrogenation), (ii) NaNO2, H2SO4, (iii) aq. NaI, I2, CHCl3, urea
4: aq. HCl / acetic acid
View Scheme
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
反应条件
1: H2 / Pd-C / ethanol
2: MeSO2Cl
3: (i) (catalytic hydrogenation), (ii) NaNO2, H2SO4, (iii) aq. NaI, I2, CHCl3, urea
4: aq. HCl / acetic acid
View Scheme
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
