双环[4.4.1]十一碳-1(10),2,4,6,8-五烯合成路线 （共 33 条）
参考文献
Scholl, Thomas; Lex, Johann; Vogel, Emanuel
Angewandte Chemie, 1982 , vol. 94, # 12 p. 924 - 925
反应条件
bromine azide in dichloromethane T=-30°C; 2 h;
参考文献
Kanomata, Nobuhiro; Kawaji, Hiroyuki; Nitta, Makoto
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 618 - 625
参考文献
Klenk,H. et al.
Chemische Berichte, 1976 , vol. 109, p. 777 - 787
反应条件
tautomerism, ΔH; Thermodynamic data;
参考文献
Journal of Physical Chemistry, , vol. 87, # 5 p. 895 - 898
反应条件
1: 38 percent / BrN3 / CH2Cl2 / 2 h / -30 °C 2: 78 percent / diethyl ether / 2 h / Ambient temperature 3: 75 percent / 48 h / Ambient temperature View Scheme
参考文献
Kanomata, Nobuhiro; Kawaji, Hiroyuki; Nitta, Makoto
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 618 - 625
反应条件
bromine; acetic acid T=20°C; 0.75 h;
参考文献
Neidlein, Richard; Constantinescu, Take
Chemische Berichte, 1989 , vol. 122, p. 1003 - 1008
反应条件
iron(III) chloride in 1,2-dichloro-ethane 1.) -30 deg C, 15 min, 2.) 20 deg C, 1 h;
参考文献
Neidlein, Richard; Constantinescu, Take
Chemische Berichte, 1989 , vol. 122, p. 1003 - 1008
反应条件
bromine 1) CH2Cl2, 0 deg C, 2) CH2Cl2, glacial acetic acid, -30 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Neidlein, Richard; Constantinescu, Take; Boese, Roland; Blaeser, Dieter
Chemische Berichte, 1988 , vol. 121, p. 1699 - 1702
反应条件
in benzene T=20°C; 1 h; further temp., solvents, reaction times; also in the presence of Lewis acids, iron; also under irradiation; also with ammonium thiocyanate as reactant; Product distribution;
参考文献
Neidlein, Richard; Constantinescu, Take
Chemische Berichte, 1989 , vol. 122, p. 1003 - 1008
反应条件
in presence of iron; AlCl3, FeCl3 or SnCl4; Product distribution;
参考文献
Neidlein, Richard; Constantinescu, Take; Kohl, Matthias
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 59, # 1-4 p. 165 - 168
