alpha-2-丙烯-1-基-苯乙醛合成路线 （共 24 条）
反应条件
diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; 1 h; Inert atmosphere;
参考文献
Joosten, Antoine; Lambert, Emilie; Vasse, Jean-Luc; Szymoniak, Jan
Organic Letters, 2010 , vol. 12, # 22 p. 5128 - 5131
反应条件
pyridinium chlorochromate in dichloromethane
18 h;
参考文献
Bloodworth, A. J.; Courtneidge, J. L.; Curtis, Richard J.; Spencer, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2951 - 2955
反应条件
sodium hydroxide; N-(N-L-γ-glutamyl-L-cysteinyl)glycine in various solvent(s)
T=20°C; UV-irradiation;
参考文献
Hartung; Kneuer; Spehar
Chemical Communications, 2001 , # 9 p. 799 - 800
反应条件
benzoylchlorobis(triphenylphosphine)palladium(II) in tetrahydrofuran
T=90°C; 48 h;
参考文献
Pri-Bar, I.; Pearlman, P. S.; Stille, J. K.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4629 - 4634
反应条件
tri-n-butyl-tin hydride in various solvent(s)
T=80°C; 0.0416667 h; microwave irradiation;
参考文献
Hartung, Jens; Daniel, Kristina; Gottwald, Thomas; Gross, Andreas; Schneiders, Nina
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 11 p. 2313 - 2322
反应条件
pyrrolidine; 1,1'-bis-(diphenylphosphino)ferrocene; bis(η3-allyl-μ-chloropalladium(II)) in methanol
T=20°C; 18 h; Inert atmosphere;
参考文献
Zhao, Xiaohu; Liu, Delong; Guo, Hui; Liu, Yangang; Zhang, Wanbin
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19354 - 19357
反应条件
2,2'-azo-bisisobutyronitrile in various solvent(s)
T=80°C; 0.0416667 h; microwave irradiation;
参考文献
Hartung, Jens; Daniel, Kristina; Gottwald, Thomas; Gross, Andreas; Schneiders, Nina
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 11 p. 2313 - 2322
反应条件
2,2'-azo-bisisobutyronitrile in various solvent(s)
T=80°C; 0.0416667 h; microwave irradiation;
参考文献
Hartung, Jens; Daniel, Kristina; Gottwald, Thomas; Gross, Andreas; Schneiders, Nina
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 11 p. 2313 - 2322
反应条件
1: 98 percent / CH3CO3H / 0 °C
2: 74 percent / HgO, BF3*OEt2 / tetrahydrofuran; H2O
View Scheme
参考文献
Block,E.; Ahmad,S.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6731
反应条件
tetrakis(triphenylphosphine) palladium(0); benzoic acid in toluene
T=60°C; Tsuji-Trost α-allylation; 12 h; Inert atmosphere;
参考文献
Jiang, Gaoxi; List, Benjamin
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1667 - 1670
