9H-吡啶并[2,3-b]吲哚合成路线 （共 33 条）
反应条件
1,10-phenanthroline; carbon monoxide; palladium diacetate in N,N-dimethyl-formamide T=140°C; P=3102.89 Torr; 16 h;
参考文献
Organic Letters, , vol. 6, # 4 p. 533 - 535
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; PCy3∙HBF4 in N,N-dimethyl acetamide; o-xylene T=145°C; 16 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 8 p. 3152 - 3155
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane T=180°C; 0.166667 h; Microwave irradiationsealed tube;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 16 p. 2653 - 2660
反应条件
1: With sodium t-butanolate; palladium diacetate; triphenylphosphine in o-xylene T=120°C; 3 h; Inert atmosphere; 2: With palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; tri-cyclo-hexyl-phosphine in isobutyramide; o-xylene T=150°C; 12 h;
参考文献
WO2012/145173 A1, ;
Page/Page column 52-53 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; aniline; triphenylphosphine; sodium t-butanolate; palladium diacetate in dichloromethane; isobutyramide; o-xylene
反应条件
1: With palladium diacetate; triphenylphosphine; sodium t-butanolate in o-xylene T=120°C; 3 h; 2: With palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; PCy3∙HBF4 in o-xylene; dimethyl amine
参考文献
WO2013/42035 A1, ;
Page/Page column 18-19 ;
反应条件
polyphosphoric acid T=160 - 175°C; 3 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 8 p. 1948 - 1951
反应条件
hydrogen bromide in ethanol T=80 - 100°C; 1.5 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , p. 926 - 932
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 16, # 9 p. 1227 - 1234
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2626,2629
反应条件
1: 77 percent / 2 h / 150 - 160 °C 2: 36 percent / PPA / 2 h / 150 - 160 °C View Scheme
参考文献
Synlett, , # 14 p. 2237 - 2241
