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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
L(-)岩藻糖
合成路线
（共 27 条）
79-06-1
丙烯酰胺
→
反应条件
2438-80-4
L(-)岩藻糖
反应条件
in water; isopropyl alcohol
参考文献
US5891862 A1, ;
1202249-78-2
+
66347-26-0
→
反应条件
2438-80-4
L(-)岩藻糖
+
1202249-91-9
反应条件
1: in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=20 - 40°C; Staudinger ligation; Inert atmosphere; 2: With water in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=40°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 33 p. 5744 - 5751
7658-10-8
6-脱氧-L-太洛醣
→
反应条件
2438-80-4
L(-)岩藻糖
反应条件
molybdenum(VI) oxide in water 9.5 h; Reflux; Reagent/catalyst;
参考文献
US2013/72675 A1, ;
Paragraph 0040; 0041; 0042 ;
1202249-77-1
+
66347-26-0
→
反应条件
2438-80-4
L(-)岩藻糖
+
1202249-90-8
反应条件
1: in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=20 - 40°C; Staudinger ligation; Inert atmosphere; 2: With water in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=40°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 33 p. 5744 - 5751
1202249-75-9
+
66347-26-0
→
反应条件
2438-80-4
L(-)岩藻糖
反应条件
1: in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=20 - 40°C; Staudinger ligation; Inert atmosphere; 2: With water in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=40°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 33 p. 5744 - 5751
1202249-76-0
+
66347-26-0
→
反应条件
2438-80-4
L(-)岩藻糖
+
1202249-89-5
反应条件
1: in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=20 - 40°C; Staudinger ligation; Inert atmosphere; 2: With water in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=40°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 33 p. 5744 - 5751
1202249-74-8
+
66347-26-0
→
反应条件
2438-80-4
L(-)岩藻糖
+
1202249-87-3
反应条件
1: in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=20 - 40°C; Staudinger ligation; Inert atmosphere; 2: With water in N,N'-dimethyl-N,N'-propyleneurea; N,N-dimethyl acetamide T=40°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 33 p. 5744 - 5751
33639-77-9
→
反应条件
2438-80-4
L(-)岩藻糖
反应条件
1: 42 percent / tetraethylammonium bromide; 4 Angstroem molecular sieves / CH2Cl2 / 24 h / 20 °C 2: 71 percent / H2 / Pd-C / ethanol 3: H2 / Pd-C / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 12 p. 2421 - 2439
169532-17-6
乙基2,3,4-三-O-苄基-1-硫代-alpha,beta-L-吡喃岩藻糖苷
→
反应条件
2438-80-4
L(-)岩藻糖
反应条件
1: CH2Cl2 / 0.33 h / 0 °C 2: 42 percent / tetraethylammonium bromide; 4 Angstroem molecular sieves / CH2Cl2 / 24 h / 20 °C 3: 71 percent / H2 / Pd-C / ethanol 4: H2 / Pd-C / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 12 p. 2421 - 2439
204588-90-9
→
反应条件
2438-80-4
L(-)岩藻糖
+
782-27-4
反应条件
hydrogen; palladium on activated charcoal in ethanol Hydrogenolysis;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 12 p. 2421 - 2439
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