反应条件
1: 38 percent / HNO3 (d= 1,40), H2SO4 (d = 1,83)
2: 97 percent / H2, aq. HCl / 10percent Pd/C / 22800 Torr / Ambient temperature
4: 1.) 2n HCl, NaNO2, 2.) 50percent H3PO2 / 1.) H2O, -5 deg C, 1.5 h, 2.) 24 h, 0 deg C
5: 68 percent / Mg / diethyl ether / 8 h / autoclave
View Scheme
参考文献
Kaliakoudas, Dimitrios; Eugster, Conrad Hans; Rueedi, Peter
Helvetica Chimica Acta, 1990 , vol. 73, # 1 p. 48 - 62
