2-[(2-甲基-2-丙基)二硫基]吡啶合成路线 （共 49 条）
反应条件
4-(N,N-dimethlyamino)pyridine; Fonderma in benzene
T=80°C; 1 h; var. of thiol, reagent; Product distribution;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Chemical Communications, 1984 , # 12 p. 774 - 775
反应条件
in dichloromethane
T=0°C; 0.333333 h; Irradiation; Product distribution;
参考文献
Blom, Petra; Xiang, Alan X.; Kao, David; Theodorakis, Emmanuel A.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 5 p. 727 - 736
反应条件
1: 80 percent / I2 / 16 h / 100 °C
2: oxalyl chloride / benzene / 2 h / Ambient temperature
3: CH2Cl2 / 2 h / Heating
4: benzene / 2 h / 80 °C / Irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Duggan, Sandhya A. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1509 - 1518
反应条件
1: dimethylsulfoxide / 100 °C
2: 80 percent / I2 / 16 h / 100 °C
3: oxalyl chloride / benzene / 2 h / Ambient temperature
4: CH2Cl2 / 2 h / Heating
5: benzene / 2 h / 80 °C / Irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Duggan, Sandhya A. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1509 - 1518
反应条件
1: oxalyl chloride / benzene / 2 h / Ambient temperature
2: CH2Cl2 / 2 h / Heating
3: benzene / 2 h / 80 °C / Irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Duggan, Sandhya A. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1509 - 1518
反应条件
oxalyl dichloride
1.) benzene, 18 h, 2.) chlorobenzene, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1603 - 1612
反应条件
4-(N,N-dimethlyamino)pyridine
benzene, 1.) room temp., 18 h, 2. ) 80 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1603 - 1612
反应条件
in benzene
T=80°C; 2 h; Irradiation;
参考文献
Beckwith, Athelstan L. J.; Duggan, Sandhya A. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1509 - 1518
反应条件
in dichloromethane
Decomposition; 1.83333 h; Photolysiscooling;
参考文献
Wu; Begley
Organic letters, 2000 , vol. 2, # 10 p. 1345 - 1348
反应条件
in benzene
6 h; Irradiation;
参考文献
Esker, John L.; Newcomb, Martin
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4933 - 4940
