2-[(2-甲基-2-丙基)二硫基]吡啶合成路线 （共 49 条）
反应条件
in dichloromethane
Irradiation;
参考文献
Barton, Derek H.R.; Lacher, Brigitte; Zard, Samir Z.
Tetrahedron, 1987 , vol. 43, # 19 p. 4321 - 4328
反应条件
1-hydroxy-2(1H)-pyridinethione in benzene
T=80°C; 3 h;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
Decomposition; Photolysis;
参考文献
Wu; Begley
Organic letters, 2000 , vol. 2, # 10 p. 1345 - 1348
反应条件
in dichloromethane
T=0°C; 0.5 h;
参考文献
Hunter, Roger; Caira, Mino; Stellenboom, Nashia
Journal of Organic Chemistry, 2006 , vol. 71, # 21 p. 8268 - 8271
参考文献
Barton, Derek H.R.; Crich, David
Tetrahedron Letters, 1985 , vol. 26, # 6 p. 757 - 760
反应条件
Na salt of N-hydroxypyridine-2-thione in chlorobenzene
1.5 h; HeatingReaction with various acyl chlorides, and the effect of excess of 2-carbethoxy-3-t-butylthioprop-1-ene.; Product distribution;
参考文献
Barton, Derek H. R.; Crich, David
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2787 - 2790
反应条件
oxygen; 2-methylpropane-2-thiol in toluene
0.25 h; Ambient temperatureIrradiationadding 15 min; Yield given;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
oxygen; 2-methylpropane-2-thiol in toluene
0.25 h; Ambient temperatureIrradiation; Yield given. Title compound not separated from byproducts;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
4-(N,N-dimethlyamino)pyridine
1.) pyridine, room temp., 18 h, 2.) benzene, 80 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1603 - 1612
反应条件
oxalyl dichloride
1.) benzene, room temp., 16 h, 2.) chlorobenzene, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1603 - 1612
