3,7-二甲基-1,6-辛二烯合成路线 (共 77 条)
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 27, # 5 p. 601 - 602
反应条件
hydrogen; η6-(methyl benzoate)tricarbonylchromium(0) T=150°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 170 - 171
反应条件
hydrogen; lt;Co(SCN)(PPh3)3gt; in ethylene glycol dimethyl ether T=17°C; P=760 Torr; rate of H2 uptake;; Product distributionMechanism;
参考文献
Nakayama; Kanai
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 16 - 22
反应条件
1: Ni(nBu3P)2Cl2 / propan-2-ol / 8 h / 80 °C 2: H2 / Cr(CO)3(PhCO2Me) / 150 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 170 - 171
反应条件
1: Pd(nBu3P)2Cl2 / propan-2-ol; methanol 2: H2 / Cr(CO)3(PhCO2Me) / 150 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 170 - 171
反应条件
ethanol; hydrazine hydrate anschliessendes Erhitzen mit Natriumaethylat auf 210grad;
参考文献
Helvetica Chimica Acta, , vol. 34, p. 1577,1584
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 29, p. 116 - 121
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 29, p. 116 - 121
反应条件
tri-n-butyl-tin hydride T=25°C; P=9750780 Torr; 24 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 371, p. C4 - C8
反应条件
triethylamine in tetrahydrofuran T=50°C; 8 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 36, p. 1455 - 1461