3,7-二甲基-1,6-辛二烯合成路线 (共 77 条)
反应条件
BF3·2HOAc T=-25°C; 1 equivalent (AcOH)2*BF3;
参考文献
Pandy-Szekeres, David; Deleris, Gerard; Picard, Jean-Paul; Pillot, Jean-Paul; Calas, Raymond
Tetrahedron Letters, 1980 , vol. 21, p. 4267 - 4270
反应条件
sodium cyanoborohydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=66°C; 44 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 21, p. 27 - 30
反应条件
polymethylhydrosiloxane; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 120 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 48, # 20 p. 3545 - 3548
反应条件
tributylphosphine; ammonium formate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane T=100°C; 1 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 922 - 924
反应条件
tributylphosphine; ammonium formate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane T=100°C; 6 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 922 - 924
反应条件
4 A molecular sieve; triphenylphosphine; tin(ll) chloride; bis-triphenylphosphine-palladium(II) chloride in toluene T=75°C; P=75006 Torr; 16 h; Product distribution; Further Variations:Pressuressubstrate/catalyst conc., reaction time;
参考文献
Tetrahedron Letters, , vol. 42, # 22 p. 3697 - 3700
反应条件
(R)-Lewis acid (SnCl4) assisted chiral Bronsted acid from (R)-binaphthol monomethyl ether in dichloromethane T=-90°C;
参考文献
Synlett, , vol. 1997, # 7 p. 758 - 760
反应条件
(R)-Lewis acid (SnCl4) assisted chiral Bronsted acid from (R)-binaphthol monomethyl ether in dichloromethane T=-90°C;
参考文献
Synlett, , vol. 1997, # 7 p. 758 - 760
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; tin(ll) chloride in toluene T=80°C; P=75006 Torr; 16 h; Further byproducts given;
参考文献
Journal of Organometalic Chemistry, , vol. 643-644, p. 12 - 18
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; tin(ll) chloride in toluene T=84°C; P=30002.4 Torr; 40 h; Further byproducts given;
参考文献
Journal of Organometalic Chemistry, , vol. 643-644, p. 12 - 18