4-甲氧基苄基对茴香酸酯合成路线 （共 22 条）
反应条件
bis(1,5-cyclooctadiene)nickel (0); SlPr in toluene T=40°C; Tishchenko reaction; 4 h; Inert atmosphere;
参考文献
Hoshimoto, Yoichi; Ohashi, Masato; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 13 p. 4668 - 4671
反应条件
[RuCl2(IiPr)(p-cymene)]; potassium hydroxide; tri-cyclo-hexyl-phosphine in 1,3,5-trimethyl-benzene T=163°C; 18 h; Inert atmosphere;
参考文献
Solvhoj, Amanda; Madsen, Robert
Organometallics, 2011 , vol. 30, # 21 p. 6044 - 6048
反应条件
C15H22Cl2N2Ru; potassium tert-butylate in toluene 24 h; Inert atmosphereReflux;
参考文献
Chen, Cheng; Zhang, Yao; Hong, Soon Hyeok
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10005 - 10010
反应条件
EtNdI in tetrahydrofuran T=65°C; 20 h;
参考文献
Yokoo, Kazuhiro; Mine, Norioko; Taniguchi, Hiroshi; Fujiwara, Yuzo
Journal of Organometallic Chemistry, 1985 , vol. 279, p. C19 - C21
反应条件
1: (4-methoxyphenyl)methanol With oxygen; caesium carbonate in α,α,α-trifluorotoluene T=100°C; 20 h; Air atmosphereIonic liquid; 2: methyl iodide With potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Oda, Yoshiro; Hirano, Koji; Satoh, Tetsuya; Kuwabata, Susumu; Miura, Masahiro
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5392 - 5394
反应条件
4-tert-butylbenzyl mercaptan; Di-n-butylmagnesium in tetrahydrofuran T=65°C; Tishchenko-Claisen Dismutation;
参考文献
Curran, Simon P.; Connon, Stephen J.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10866 - 10870
The Thiolate-Catalyzed Intermolecular Crossed Tishchenko Reaction: Highly Chemoselective Coupling of Two Different Aromatic Aldehydes, 2012 , vol. 124, # 43 p. 11024 - 11028,5
反应条件
Au-Pd/C; oxygen T=160°C; P=7500.75 Torr; 7 h;
参考文献
Kesavan, Lokesh; Tiruvalam, Ramchandra; Rahim, Mohd Hasbi Ab; Saiman, Mohd Izham Bin; Enache, Dan I.; Jenkins, Robert L.; Dimitratos, Nikolaos; Lopez-Sanchez, Jose A.; Taylor, Stuart H.; Knight, David W.; Kiely, Christopher J.; Hutchings, Graham J.
Science, 2011 , vol. 331, # 6014 p. 195 - 199
反应条件
1: thionyl chloride / dichloromethane / 2 h / 40 °C 2: triethylamine / dichloromethane / 20 °C View Scheme
参考文献
Chen, Dongyin; Xu, Chang; Deng, Jie; Jiang, Chunhuan; Wen, Xiaoan; Kong, Lingyi; Zhang, Ji; Sun, Hongbin
Tetrahedron, 2014 , vol. 70, # 11 p. 1975 - 1983
反应条件
oxygen T=80°C; pH=9; 4 h; aq. buffer;
参考文献
Saio, Daisuke; Amaya, Toru; Hirao, Toshikazu
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2177 - 2182
反应条件
18-crown-6 ether in benzene T=20°C; Reduction; silylation; addition; 20 h; Product distribution; Further Variations:SolventsTemperaturesamount of reagents, reactants;
参考文献
Bideau, Franck Le; Coradin, Thibaud; Gourier, Didier; Henique, Josette; Samuel, Edmond
Tetrahedron Letters, 2000 , vol. 41, # 27 p. 5214 - 5218
