1-(4-甲基苯基)-2-苯基乙烷-1,2-二酮合成路线 (共 60 条)
反应条件
silver hexafluoroantimonate; bis-(phenyl)-sulfoxide; gold(I) chloride in 1,2-dichloro-ethane 3 h; Reflux;
参考文献
Xu, Cheng-Fu; Xu, Mei; Jia, Yi-Xia; Li, Chuan-Ying
Organic Letters, 2011 , vol. 13, # 6 p. 1556 - 1559
反应条件
pyridinium chlorochromate in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Bhosale, Shrikar M.; Momin, Aadil A.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5327 - 5330
反应条件
N-bromosuccinmide; dimethyl sulfoxide 72 h; Ambient temperature;
参考文献
Tatsugi, Jiro; Izawa, Yasuji
Journal of Chemical Research, Miniprint, 1988 , # 11 p. 2747 - 2763
反应条件
tert.-butylhydroperoxide; [Ru2Cl(3,6-bis(1-(2-pyridylmethyl)imidazol-2-yliden-3-yl)pyridazine)(CH3CN)4](PF6)3; sodium iodide in water; acetonitrile T=20°C; 0.166667 h;
参考文献
Liu, Xiaolong; Chen, Wanzhi
Organometallics, 2012 , vol. 31, # 18 p. 6614 - 6622
反应条件
sulfuric acid in acetic acid T=118°C; 2 h;
参考文献
Krasnokutskaya; Yusubov; Filimonov; Habicher
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 7 p. 1001 - 1004
反应条件
[RuCl2(PPh3)4] in dichloromethane T=20°C;
参考文献
US2008/64872 A1, ;
Page/Page column 17 ;
US 20080064872 A1
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=50°C; Arylation; carbonylation; P=760 Torr; 10 h;
参考文献
Sakurai, Hidehiro; Tanabe, Katsuhiko; Narasaka, Koichi
Chemistry Letters, 2000 , # 2 p. 168 - 169
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in benzene 5 h; Heating;
参考文献
Vankar, Yashwant D.; Shah, Kavita; Bawa, Anita; Singh, Surendra P.
Tetrahedron, 1991 , vol. 47, # 42 p. 8883 - 8906
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Qi, Chaorong; Jiang, Huanfeng; Huang, Liangbin; Chen, Zhengwang; Chen, Huoji
Synthesis, 2011 , # 3 art. no. F17110SS, p. 387 - 396
反应条件
1,4-diaza-bicyclo[2.2.2]octane; Iron (III) nitrate nonahydrate; oxygen; copper(II) bis(trifluoromethanesulfonate); 4-methoxy-aniline in acetonitrile T=0°C; P=760.051 Torr; 16 h; chemoselective reaction;
参考文献
Su, Yijin; Sun, Xiang; Wu, Guolin; Jiao, Ning
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9808 - 9812
Angew. Chem., 2013 , p. 9990 - 9994