10H-吲哚并[3,2-b]喹啉合成路线 (共 69 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol; chloroform
P=1810.07 Torr; 12 h;
参考文献
Bastos, Dayse Dos S.; Silva, Anna C.; Albert, Andre L.M.; Barros, Wesley M.R.; Slana, Glaucia B.C.A.; Cardoso, Jari N.; Lopes, Rosangela S.C.; Lopes, Claudio C.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3144 - 3146
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Cooper; Lovell; Joule
Tetrahedron Letters, 1996 , vol. 37, # 24 p. 4283 - 4286
反应条件
sodium acetate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=180°C; Heck reaction; 0.166667 h; microwave irradiation;
参考文献
Hostyn, Steven; Maes, Bert U.W.; Van Baelen, Gitte; Gulevskaya, Anna; Meyers, Caroline; Smits, Koen
Tetrahedron, 2006 , vol. 62, # 19 p. 4676 - 4684
反应条件
pyridine hydrochloride
T=215°C;
参考文献
Arzel; Rocca; Grellier; Labaeid; Frappier; Gueritte; Gaspard; Marsais; Godard; Queguiner
Journal of Medicinal Chemistry, 2001 , vol. 44, # 6 p. 949 - 960
反应条件
sodium acetate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=130°C; 48 h;
参考文献
Hostyn, Steven; Maes, Bert U.W.; Pieters, Luc; Lemiere, Guy L.F.; Matyus, Peter; Hajos, Gyoergy; Dommisse, Roger A.
Tetrahedron, 2005 , vol. 61, # 6 p. 1571 - 1577
反应条件
sulfuric acid; iodine in methanol; benzene
T=20°C; 48 h; UV-irradiation;
参考文献
Dhanabal; Sangeetha; Mohan
Tetrahedron, 2006 , vol. 62, # 26 p. 6258 - 6263
反应条件
1: 70 percent / 5 h / 200 °C
2: 16 percent / sulfuric acid; iodine / benzene; methanol / 48 h / 20 °C / UV-irradiation
View Scheme
参考文献
Dhanabal; Sangeetha; Mohan
Tetrahedron, 2006 , vol. 62, # 26 p. 6258 - 6263
反应条件
[bis(acetoxy)iodo]benzene in tetrahydrofuran
T=20°C; 3 h;
参考文献
Ho, Tse-Lok; Jou, Der-Guey
Helvetica Chimica Acta, 2002 , vol. 85, # 11 p. 3823 - 3827
反应条件
1: aq. KOH / 240 h / 20 °C
2: diphenyl ether / 6 h / 250 °C
View Scheme
参考文献
Wright; Addae-Kyereme; Breen; Brown; Cox; Croft; Goekcek; Kendrick; Phillips; Pollet
Journal of Medicinal Chemistry, 2001 , vol. 44, # 19 p. 3187 - 3194
反应条件
1: 70 percent / PCl5 / 3 h / Heating
2: 80 percent / HCl; H2 / 10 percent Pd/C / methanol / 2 h / 760 Torr
View Scheme
参考文献
Radl; Konvicka; Vachal
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 4 p. 855 - 862