11H-10,11-二氮杂苯并[b]芴合成路线 （共 72 条）
反应条件
triphenylphosphine in diphenylether
4 h; Inert atmosphereReflux;
参考文献
Kadam, Harik.; Parvatkar, Prakasht.; Tilve, Santosh G.
Synthesis, 2012 , vol. 44, # 9 p. 1339 - 1342
反应条件
acetic acid
2 h; Heating;
参考文献
Marsais, F.; Godard, A.; Queguiner, G.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1589 - 1594
反应条件
1: 83 percent / benzene / 1 h / 20 °C
2: 16 percent / γ-terpinene / 14 h / 138 °C
View Scheme
参考文献
Shi, Chongsheng; Zhang, Quan; Wang, Kung K.
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 925 - 932
反应条件
1: 83 percent / benzene / 1 h / 20 °C
2: 16 percent / γ-terpinene / 14 h / 138 °C
View Scheme
参考文献
Shi, Chongsheng; Zhang, Quan; Wang, Kung K.
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 925 - 932
反应条件
1: acetic acid; zinc / 0.17 h / Reflux
2: hydrogenchloride; sodium nitrite / methanol; water / 20 °C / Cooling with ice
View Scheme
参考文献
Haddadin, Makhluf J.; Zerdan, Raghida M. Bou; Kurth, Mark J.; Fettinger, James C.
Organic Letters, 2010 , vol. 12, # 23 p. 5502 - 5505
反应条件
1: pyrrolidine; potassium hydroxide / methanol / 2 h / Reflux
2: acetic acid; zinc / 0.17 h / Reflux
3: hydrogenchloride; sodium nitrite / methanol; water / 20 °C / Cooling with ice
View Scheme
参考文献
Haddadin, Makhluf J.; Zerdan, Raghida M. Bou; Kurth, Mark J.; Fettinger, James C.
Organic Letters, 2010 , vol. 12, # 23 p. 5502 - 5505
反应条件
1: hydrogenchloride; iron sulphate heptahydrate / water / 90 °C
2: pyrrolidine; potassium hydroxide / methanol / 2 h / Reflux
3: acetic acid; zinc / 0.17 h / Reflux
4: hydrogenchloride; sodium nitrite / methanol; water / 20 °C / Cooling with ice
View Scheme
参考文献
Haddadin, Makhluf J.; Zerdan, Raghida M. Bou; Kurth, Mark J.; Fettinger, James C.
Organic Letters, 2010 , vol. 12, # 23 p. 5502 - 5505
反应条件
1: 85 percent / 0.17 h / 180 °C / microwave irradiation
2: 19 percent / H4P2O7 / 0.01 h / 170 °C / microwave irradiation
View Scheme
参考文献
Vera-Luque, Patricia; Alajarin, Ramon; Alvarez-Builla, Julio; Vaquero, Juan J.
Organic Letters, 2006 , vol. 8, # 3 p. 415 - 418
反应条件
1: 85 percent / 0.17 h / 180 °C / microwave irradiation
2: 19 percent / H4P2O7 / 0.01 h / 170 °C / microwave irradiation
View Scheme
参考文献
Vera-Luque, Patricia; Alajarin, Ramon; Alvarez-Builla, Julio; Vaquero, Juan J.
Organic Letters, 2006 , vol. 8, # 3 p. 415 - 418
反应条件
1: 71 percent / benzene / 20 °C
2: 86 percent / p-xylene / 5 h / 138 °C
3: 92 percent / NaOH / ethanol; H2O / 12 h / Heating
View Scheme
参考文献
Shi, Chongsheng; Zhang, Quan; Wang, Kung K.
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 925 - 932
