11H-10,11-二氮杂苯并[b]芴合成路线 （共 72 条）
反应条件
hydrogenchloride; iron; acetic acid in water
T=120°C; 24 h;
参考文献
Parvatkar, Prakash T.; Tilve, Santosh G.
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6594 - 6596
反应条件
N-bromosuccinmide
T=20°C; 4.75 h; Neat (no solvent);
参考文献
Ghorbani-Vaghei, Ramin; Malaekehpoor, Seyedeh Mina
Tetrahedron Letters, 2012 , vol. 53, # 35 p. 4751 - 4753
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; 1,8-diazabicyclo[5.4.0]undec-7-ene in trans-1,3-dioxane
T=180°C; 0.166667 h; Microwave irradiationsealed tube;
参考文献
Hostyn, Steven; Van Baelen, Gitte; Lemiere, Guy L. F.; Maes, Bert U. W.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 16 p. 2653 - 2660
反应条件
potassium tert-butylate in tetrahydrofuran
T=-40°C; 4 h;
参考文献
Miller, Marc; Vogel, Johannes C.; Tsang, William; Merrit, Andrew; Procter, David J.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 3 p. 589 - 597
反应条件
hydrogenchloride; sodium nitrite in methanol; water
T=20°C; Cooling with ice;
参考文献
Haddadin, Makhluf J.; Zerdan, Raghida M. Bou; Kurth, Mark J.; Fettinger, James C.
Organic Letters, 2010 , vol. 12, # 23 p. 5502 - 5505
反应条件
PPA
1.) 110-150 deg C, 30 min, 2.) 150-200, 20 min;
参考文献
Peczynska-Czoch; Pognan; Kaczmarek; Boratynski
Journal of Medicinal Chemistry, 1994 , vol. 37, # 21 p. 3503 - 3510
反应条件
sulfuric acid; iodine in methanol; benzene
T=20°C; 48 h; UV-irradiation;
参考文献
Dhanabal; Sangeetha; Mohan
Tetrahedron, 2006 , vol. 62, # 26 p. 6258 - 6263
反应条件
sodium hydroxide in ethanol; water
desilylation; 12 h; Heating;
参考文献
Shi, Chongsheng; Zhang, Quan; Wang, Kung K.
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 925 - 932
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane
Heating;
参考文献
Sundaram; Venkatesh; Syam Kumart; Ila; Junjappa
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5760 - 5762
反应条件
HZSM-5 zeolite
T=350°C; P=0.2 Torr; Inert atmosphere;
参考文献
Pelmus, Marius; Popescu, Angela; Teodoru, Beatrice-Anamaria; Istrati, Daniela; Draghici, Constantin; Mihaiescu, Dan; Badea, Florin
Revue Roumaine de Chimie, 2012 , vol. 57, # 11 p. 965 - 970
