叔丁氧羰基-L-谷氨酸1叔丁脂合成路线 （共 26 条）
反应条件
lithium hydroxide in tetrahydrofuran; water
参考文献
More, Swati S.; Vince, Robert
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 13 p. 3793 - 3797
反应条件
palladium on activated charcoal; hydrogen in tetrahydrofuran 20 h;
参考文献
Ohshima, Takashi; Gnanadesikan, Vijay; Shibuguchi, Tomoyuki; Fukuta, Yuhei; Nemoto, Tetsuhiro; Shibasaki, Masakatsu
Journal of the American Chemical Society, 2003 , vol. 125, # 37 p. 11206 - 11207
反应条件
lithium hydroxide in tetrahydrofuran T=0°C; 0.25 h;
参考文献
Avent, Anthony G.; Duggan, Heather M. E.; Young, Douglas W.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 12 p. 2327 - 2332
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Catterick, David; Pritchard, Garcth J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 855 - 866
反应条件
1: 97 percent / TMSCl / 20 °C 2: 91 percent / Na2CO3 / dioxane; H2O 3: 94 percent / DCC; DMAP / CH2Cl2 4: 84 percent / LiOH / tetrahydrofuran; H2O View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 13 p. 3793 - 3797
反应条件
Candida antarctica lipase; phosphate buffer in methanol; hexane T=37°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 22 p. 8730 - 8733
反应条件
1: 43 percent / (S,S)-[(4-MeBn)2N(1+)(Me)CH2]2-dioxolane-2,2-di-Pr*2BF4(1-); Cs2CO3 / chlorobenzene / 10 h / -30 °C 2: 93 percent / Pd/C; H2 / tetrahydrofuran / 20 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 37 p. 11206 - 11207
反应条件
1: 89 percent / H2, 1 M methanolic HCl / 5percent Pd/C / 8 h 3: aq. NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 15 p. 6646 - 6651
反应条件
2: aq. NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 15 p. 6646 - 6651
反应条件
1: 94 percent / DCC; DMAP / CH2Cl2 2: 84 percent / LiOH / tetrahydrofuran; H2O View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 13 p. 3793 - 3797
