3,5-二乙酰基-2,6-二甲基吡啶合成路线 (共 16 条)
反应条件
silica gel; p-toluenesulfonyl chloride; sodium nitrite 0.0222222 h; microwave irradiation;
参考文献
Niknam, Khodabakhsh; Zolfigol, Mohammah Ali; Rabani, Farideh
Heterocyclic Communications, 2006 , vol. 12, # 3-4 p. 183 - 186
反应条件
tetrachlorosilane; water; silica gel; sodium nitrite in dichloromethane T=20°C; 0.75 h;
参考文献
Zolfigol, Mohammad Ali; Shirini, Farhad; Ghorbani Choghamarani, Arash; Mohammadpoor-Baltork, Iraj
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 8 p. 1709 - 1715
反应条件
oxygen in chloroform 6 h; UV-irradiation;
参考文献
Memarian, Hamid R.; Sadeghi, Majid M.; Momeni, Ahmad R.; Doepp, Dietrich
Monatshefte fur Chemie, 2002 , vol. 133, # 5 p. 661 - 667
反应条件
1: aq. NH4OAc / H2O / 1.5 h / Heating 2: KMnO4; aq. AcOH / 2 h / Heating View Scheme
参考文献
Synthesis, , # 14 art. no. F02305SS, p. 2379 - 2383
反应条件
oxygen in acetonitrile T=150°C; P=7500.75 Torr; 0.5 h; Microwave irradiationUV-irradiation;
参考文献
Australian Journal of Chemistry, , vol. 62, # 1 p. 51 - 57
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile 0.0138889 h; Microwave irradiation;
参考文献
Memarian, Hamid R.; Ghazaie, Marieh; Mehneh, Somayeh Kakhki
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2009 , vol. 64, # 10 p. 1187 - 1192
反应条件
oxygen in chloroform 7 h; UV-irradiation;
参考文献
Memarian, Hamid R.; Sadeghi, Majid M.; Momeni, Ahmad R.; Doepp, Dietrich
Monatshefte fur Chemie, 2002 , vol. 133, # 5 p. 661 - 667
反应条件
ammonia; water T=25°C;
参考文献
Chemische Berichte, , vol. 30, p. 2297
DE79863 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 1134
Justus Liebigs Annalen der Chemie, , vol. 297, p. 57
Chemische Berichte, , vol. 26, p. 2731
反应条件
1: aq. NH3 / ethanol / 7 h / Heating 2: 88 percent / O2 / CHCl3 / 6 h / UV-irradiation View Scheme
参考文献
Monatshefte fur Chemie, , vol. 133, # 5 p. 661 - 667
反应条件
in acetonitrile 6 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 28, # 9 p. 1054 - 1059
Khimiya Geterotsiklicheskikh Soedinenii, , # 9 p. 1243 - 1249