2-溴-3-甲氧基-6-甲基吡啶合成路线 （共 7 条）
反应条件
potassium carbonate in acetone Heating;
参考文献
Ross Kelly; Lang, Fengrui
Tetrahedron Letters, 1995 , vol. 36, # 30 p. 5319 - 5322
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Kelly, T. Ross; Lang, Fengrui
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4623 - 4633
反应条件
1: Br2 / pyridine / 77 h / Ambient temperature 2: 88 percent / K2CO3 / acetone / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 14 p. 4623 - 4633
反应条件
potassium permanganate in water T=90°C; 3 h;
参考文献
Kelly, T. Ross; Lang, Fengrui
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4623 - 4633
反应条件
in dichloromethane; water; ethyl acetate; acetonitrile
参考文献
Maxia Pharmaceuticals, Inc.
Patent: US6515003 B1, 2003 ;
反应条件
1: 77 percent / KMnO4 / H2O / 3 h / 90 °C 2: Et3N, DMAP / CH2Cl2 / 2 h / Ambient temperature 3: 98 percent / AlCl3, NaCl / 0.03 h / 150 °C View Scheme
参考文献
Kelly, T. Ross; Lang, Fengrui
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4623 - 4633
反应条件
1: 77 percent / KMnO4 / H2O / 3 h / 90 °C 2: Et3N, DMAP / CH2Cl2 / 2 h / Ambient temperature 3: 93 percent / AlCl3 / CH2Cl2 / 48 h / Heating View Scheme
参考文献
LUMIPHORE, INC.; MAGDA, Darren; XU, Jide; BUTLIN, Nathaniel, G.
Patent: WO2014/78690 A1, 2014 ;
反应条件
1: 77 percent / KMnO4 / H2O / 3 h / 90 °C 2: Et3N, DMAP / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
LUMIPHORE, INC.; MAGDA, Darren; XU, Jide; BUTLIN, Nathaniel, G.
Patent: WO2014/78690 A1, 2014 ;
