3,3',4,4'-联苯四羧酸二酐合成路线 （共 14 条）
反应条件
acetic anhydride; acetic acid
参考文献
UBE Industries, Ltd.
Patent: US3940426 A1, 1976 ;
参考文献
Journal of the Chemical Society, , vol. 105, p. 2480
反应条件
1,2-dichloro-1,1,2,2-tetramethyldisilane; bis(benzonitrile)palladium(II) dichloride; bis(1,1-diphenylphosphino)methane in 1,3,5-trimethyl-benzene 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 55, # 20 p. 5430 - 5432
反应条件
bis(benzonitrile)palladium(II) dichloride; bis(1,1-diphenylphosphino)methane in 1,3,5-trimethyl-benzene 18 h; Heatingvariation of condition; other aromatic acid chlorides; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 55, # 20 p. 5430 - 5432
反应条件
1: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 2: hydrogenchloride / water 3: acetic anhydride / |Heating View Scheme
反应条件
1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / methanol; toluene / 4 h / 80 °C / |Inert atmosphere 2: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 3: hydrogenchloride / water 4: acetic anhydride / |Heating View Scheme
反应条件
1: hydrogenchloride / water 2: acetic anhydride / |Heating View Scheme
反应条件
1: water / 2 h / 100 °C 2: hydrogenchloride / water 3: acetic anhydride / |Heating View Scheme
反应条件
1: palladium 10 on activated carbon / 6 h / 250 °C / |Inert atmosphere 2: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 3: hydrogenchloride / water 4: acetic anhydride / |Heating View Scheme
反应条件
1: lanthanum-deposited zeolite / 2 h / 180 °C / |Autoclave; |Inert atmosphere 2: palladium 10 on activated carbon / 6 h / 250 °C / |Inert atmosphere 3: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 4: hydrogenchloride / water 5: acetic anhydride / |Heating View Scheme
