5-甲基嘧啶-2,4,6(1H,3H,5H)-三酮合成路线 (共 34 条)
反应条件
sodium methylate in methanol 16 h; Reflux;
参考文献
Puig-De-La-Bellacasa, Raimon; Gimenez, Laura; Pettersson, Sofia; Pascual, Rosalia; Gonzalo, Encarna; Este, Jose A.; Clotet, Bonaventura; Borrell, Jose I.; Teixido, Jordi
European Journal of Medicinal Chemistry, 2012 , vol. 54, p. 159 - 174
反应条件
hydrogen; platinum on activated charcoal in methanol Knoevenagel condensation; P=2585.74 Torr; 20 h;
参考文献
Jursic, Branko S.; Neumann, Donna M.
Tetrahedron Letters, 2001 , vol. 42, # 25 p. 4103 - 4107
反应条件
hydrogenchloride; zinc in water T=20°C; 0.5 h;
参考文献
Jursic, Branko S.; Stevens, Edwin D.
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2203 - 2210
反应条件
hydrogenchloride; sodium; urea in ethanol; water
参考文献
Ciba-Geigy Corporation
Patent: US4741760 A1, 1988 ;
反应条件
Saline; Nitrous oxide in water Ambient temperatureIrradiation; Further byproducts given;
参考文献
Kagiya, Tsutomu; Kimura, Ryoji; Komuro, Chikara; Sakano, Koichi; Nishimoto, Sei-ichi
Chemistry Letters, 1983 , p. 1471 - 1474
反应条件
4-nitro-1H-imidazole in water IrradiationpH=7.0+/-0.1; Further byproducts given;
参考文献
Wada, Takeshi; Ide, Hiroshi; Nishimoto, Sei-ichi; Kagiya, Tsutomu
Chemistry Letters, 1982 , p. 1041 - 1044
反应条件
Saline; oxygen in water Ambient temperatureIrradiation; Further byproducts given;
参考文献
Kagiya, Tsutomu; Kimura, Ryoji; Komuro, Chikara; Sakano, Koichi; Nishimoto, Sei-ichi
Chemistry Letters, 1983 , p. 1471 - 1474
反应条件
sodium formate in water Irradiation;
参考文献
Nishimoto, Sei-ichi; Ide, Hiroshi; Nakamichi, Kikumi; Otsuki, Nobuaki; Kagiya, Tsutomu
Chemistry Letters, 1983 , p. 1441 - 1444
参考文献
Fahr, Egon; Fecher, Peter; Roth, Georg; Wuestenfeld, Peter
Angewandte Chemie, 1980 , vol. 92, # 10 p. 858 - 859
反应条件
1: H2O / Irradiation 2: O2 / Irradiation View Scheme
参考文献
Fahr, Egon; Fecher, Peter; Roth, Georg; Wuestenfeld, Peter
Angewandte Chemie, 1980 , vol. 92, # 10 p. 858 - 859