(2,2-二氯环丙基)苯合成路线 （共 37 条）
反应条件
1: dimethylformamide / 0.5 h / -20 °C
2: 1 h / 58 - 62 °C
View Scheme
参考文献
Crossland, Ingolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 4 p. 310 - 312
反应条件
in N,N-dimethyl-formamide
T=-20°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Crossland, Ingolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 4 p. 310 - 312
反应条件
potassium hydroxide
T=78°C; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Kostikov; Varakin; Molchanov; Ogloblin
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 1 p. 25 - 30
反应条件
1: dimethylformamide / 0.5 h / -20 °C
2: dimethylformamide / 1 h / 20 °C
View Scheme
参考文献
Crossland, Ingolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 4 p. 310 - 312
反应条件
1: OH(1-) / Heating
2: aq. formic acid
View Scheme
参考文献
Thompson, Charles D.; Kinter, Michael T.; Macdonald, Timothy L.
Chemical Research in Toxicology, 1996 , vol. 9, # 8 p. 1225 - 1229
反应条件
potassium tert-butylate in tetrahydrofuran
T=12°C;
参考文献
Ding, Mei-Fang; Lee, Chuan-Chen; Lin, Lian-Chun; Lin, Shaw-Tao
Journal of the Chinese Chemical Society, 2014 , vol. 61, # 2 p. 285 - 289
反应条件
aluminium trichloride
参考文献
Buddrus,J.
Chemische Berichte, 1968 , vol. 101, p. 4152 - 4162
