(2,2-二氯环丙基)苯合成路线 (共 37 条)
反应条件
potassium hydroxide; tetrabutylammomium bromide; 1,3,5-trimethyl-benzene in dichloromethane T=40°C; 6 h;
参考文献
Nicolas, Cyril; Lacour, Jerome
Organic Letters, 2006 , vol. 8, # 19 p. 4343 - 4346
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran; 1,2-dichloro-ethane T=0°C; 1 h;
参考文献
Chien, Ching-Ting; Tsai, Chia-Chung; Tsai, Chi-Hui; Chang, Tsai-Yuan; Tsai, Ping-Kuei; Wang, Ying-Chuan; Yan, Tu-Hsin
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4324 - 4327
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water 3 h; Ambient temperature;
参考文献
Jonczyk, A.; Balcerzak, P.
Tetrahedron Letters, 1989 , vol. 30, # 35 p. 4697 - 4700
反应条件
sodium hydroxide; tetrabutyl-ammonium chloride T=0°C; 0.25 h;
参考文献
Castedo, Luis; Castro, Jose L.; Riguera, Ricardo
Heterocycles, 1982 , vol. 19, # 2 p. 209 - 212
反应条件
potassium hydroxide; 18-crown-6 ether in benzene T=40°C;
参考文献
Singleton, Daniel A.; Wang, Zhihong
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 2033 - 2036
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water 3 h; Ambient temperature;
参考文献
Jonczyk, A.; Balcerzak, P.
Tetrahedron Letters, 1989 , vol. 30, # 35 p. 4697 - 4700
反应条件
sodium methylate in tetrahydrofuran T=-10°C;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 188, # 1-3 p. 106 - 110
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 18, # 16-17 p. 2117 - 2122
反应条件
in benzene T=20°C; Irradiationphotolysis;
参考文献
Ziegler, Christopher J.; Suslick, Kenneth S.
Journal of Organometallic Chemistry, 1997 , vol. 528, # 1-2 p. 83 - 90
反应条件
in tetrahydrofuran; toluene T=-78 - 20°C;
参考文献
Kimura, Tsutomu; Tsuru, Takahiro; Momochi, Hitoshi; Satoh, Tsuyoshi
Heteroatom Chemistry, 2013 , vol. 24, # 2 p. 131 - 137