P,P-二苯基-N-(三苯基膦)-亚膦酰胺合成路线 （共 2 条）
反应条件
1: amino(triphenyl)phosphonium chloride With n-butyllithium in tetrahydrofuran; hexane T=-20°C; 0.5 h; 2: chloro-diphenylphosphine T=-20 - 25°C; Further stages.;
参考文献
Taillefer, Marc; Rahier, Nicolas; Hameau, Aurelien; Volle, Jean-Noel
Chemical Communications, 2006 , # 30 p. 3238 - 3239
反应条件
1: water / 1 h / 0 °C / |Inert atmosphere; |Schlenk technique 2: methanol / 1 h / 20 °C / |Inert atmosphere; |Schlenk technique 3: anhydrous propionitrile View Scheme
参考文献
Bolli, Christoph; Gellhaar, Jorit; Jenne, Carsten; Kessler, Mathias; Scherer, Harald; Seeger, Helene; Uzun, Rabiya
Dalton Transactions, 2014 , vol. 43, # 11 p. 4326 - 4334
