1-(1-羟基环己基)过氧环己烷-1-醇合成路线 （共 49 条）
反应条件
1: aqueous H2O2
2: copper (II)-sulfate
View Scheme
参考文献
Criegee; Schnorrenberg; Becke
Justus Liebigs Annalen der Chemie, 1949 , vol. 565, p. 7,17
反应条件
chlorosulfonic acid in acetic acid
T=20°C; 0.5 h;
参考文献
Miura, Masahiro; Ikegami, Akio; Nojima, Masatomo; Kusabayashi, Shigekazu; McCullough, Kevin J.; Walkinshaw, Malcolm D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1657 - 1664
反应条件
beim Erwaermen des Reaktionsprodukts mit Methanol und wenig Toluol-4-sulfonsaeure;
参考文献
Payne; Smith
Journal of Organic Chemistry, 1958 , vol. 23, p. 1066
反应条件
2-hydroxy-1,3-isoindolinedione; ammonia; water in acetonitrile
T=55°C; P=760.051 Torr; 12 h; Product distribution / selectivity;
参考文献
Ishii, Yasutaka; Nakano, Tatsuya
Patent: US2003/204084 A1, 2003 ;
Location in patent: Page/Page column 13 ;
反应条件
2-hydroxy-1,3-isoindolinedione; ammonia in acetonitrile
T=55°C; P=760.051 Torr; 12 h; Product distribution / selectivity;
参考文献
Ishii, Yasutaka; Nakano, Tatsuya
Patent: US2003/204084 A1, 2003 ;
Location in patent: Page/Page column 13 ;
反应条件
chlorosulfonic acid; WO3 in dichloromethane
T=25°C; 5 h;
参考文献
Fujisaka, Tomohiro; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1031 - 1039
反应条件
Nafion in n-heptane
T=25°C; 4 h; Product distribution / selectivity;
参考文献
Daicel Chemical Industries, Ltd.
Patent: EP2123646 A1, 2009 ;
Location in patent: Page/Page column 27 ;
反应条件
hexafluoroisopropyl alcohol
T=25°C; 4 h; Product distribution / selectivity;
参考文献
Daicel Chemical Industries, Ltd.
Patent: EP2123646 A1, 2009 ;
Location in patent: Page/Page column 25-26 ;
反应条件
chlorosulfonic acid in acetic acid
T=20°C; 2 h;
参考文献
Miura, Masahiro; Ikegami, Akio; Nojima, Masatomo; Kusabayashi, Shigekazu; McCullough, Kevin J.; Walkinshaw, Malcolm D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1657 - 1664
