2-二苯基磷-2'-(N,N-二甲氨基)联苯合成路线 （共 9 条）
反应条件
in tetrahydrofuran T=20°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Korte, Nicholas J.; Stepanova, Valeria A.; Smoliakova, Irina P.
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 356 - 362
反应条件
diisobutylaluminium hydride in various solvent(s) T=125°C; 15 h;
参考文献
Busacca, Carl A.; Raju, Ravinder; Grinberg, Nelu; Haddad, Nizar; James-Jones, Paul; Lee, Heewon; Lorenz, Jon C.; Saha, Anjan; Senanayake, Chris H.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1524 - 1531
反应条件
in tetrahydrofuran T=20°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Journal of Organometallic Chemistry, , vol. 745-746, p. 356 - 362
反应条件
1: 92 percent / NaOAc / Pd(OAc)2 / N,N-dimethyl-acetamide / 72 h / 130 °C 2: 100 percent / H2O2 / methanol / 1 h / 20 °C 3: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C 4: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 19 p. 4159 - 4168
反应条件
1: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C 2: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 19 p. 4159 - 4168
反应条件
1: 65 percent / 1,3-bis(diphenylphosphino)propane; (i-Pr)2NEt / Pd(dba)2 / toluene / 96 h / 120 °C 2: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C 3: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 19 p. 4159 - 4168
反应条件
1: 92 percent / NaOAc / Pd(OAc)2 / N,N-dimethyl-acetamide / 72 h / 130 °C 2: 100 percent / H2O2 / methanol / 1 h / 20 °C 3: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C 4: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 19 p. 4159 - 4168
反应条件
1: 100 percent / H2O2 / methanol / 1 h / 20 °C 2: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C 3: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 19 p. 4159 - 4168
反应条件
1: tetrahydrofuran / 18 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: tetrahydrofuran / 18 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 745-746, p. 356 - 362
