2-(4-甲氧基苯基)-1,3-二氧戊环合成路线 (共 29 条)
反应条件
zinc(II) tetrahydroborate
参考文献
Fukase; Aoki; Kinoshita; Suda; Kurosawa; Zahringer; Rietschel; Kusumoto
Tetrahedron Letters, 1995 , vol. 36, # 47 p. 8645 - 8648
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether
T=30°C; Reduction; 12 h;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether
7 h; Heating; Yield given. Yields of byproduct given;
参考文献
Shaozu, Wu; Yulan, Zhang; Tianhui, Ren
Gazzetta Chimica Italiana, 1991 , vol. 121, # 9 p. 445 - 447
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether
12 h; Heating; Title compound not separated from byproducts;
参考文献
Shaozu, Wu; Yin, Chen; Yulan, Zhang
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 5 p. 421 - 424
反应条件
diiodo monosilane in dichloromethane
0.0333333 h; Ambient temperature;
参考文献
Keinan, E.; Perez, D.; Sahai, M.; Shvily, R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2927 - 2938
反应条件
1: triethoxymethane; pyridinium hydrobromide perbromide / 1,2-dichloro-ethane / 2 h / 50 °C
2: 97 percent / triethoxymethane; pyridinium hydrobromide perbromide / 1,2-dichloro-ethane / 2 h / 50 °C
View Scheme
参考文献
Aoyama, Tadashi; Takido, Toshio; Kodomari, Mitsuo
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 1989 - 1992
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
1: 86 percent / kaolinitic clay / Heating
2: 76 percent / Heating; kaolinitic clay
View Scheme
参考文献
Jnaneshwara; Barhate; Sudalai; Deshpande; Wakharkar; Gajare; Shingare; Sukumar
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 965 - 968
反应条件
3,3-dimethyldioxirane in acetone
T=25°C; Kinetics;
参考文献
Baumstark; Kovac, Franci; Vasquez, Pedro C.
Heterocyclic Communications, 2002 , vol. 8, # 1 p. 9 - 12